6,6'-dideoxy-6,6'-di(monoheptaminoacetyl)amino-2,2',3,3',4,4'-hexa-O-benzyl-α-D-trehalose

Base Information

Chemical Name:6,6'-dideoxy-6,6'-di(monoheptaminoacetyl)amino-2,2',3,3',4,4'-hexa-O-benzyl-α-D-trehalose
CAS No.:827026-07-3
Molecular Formula:C₇₂H₉₄N₄O₁₁
Molecular Weight:1191.56
Hs Code.:

Synonyms:6,6'-dideoxy-6,6'-di(monoheptaminoacetyl)amino-2,2',3,3',4,4'-hexa-O-benzyl-α-D-trehalose

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Chemical Property of 6,6'-dideoxy-6,6'-di(monoheptaminoacetyl)amino-2,2',3,3',4,4'-hexa-O-benzyl-α-D-trehalose

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Technology Process of 6,6'-dideoxy-6,6'-di(monoheptaminoacetyl)amino-2,2',3,3',4,4'-hexa-O-benzyl-α-D-trehalose

There total 5 articles about 6,6'-dideoxy-6,6'-di(monoheptaminoacetyl)amino-2,2',3,3',4,4'-hexa-O-benzyl-α-D-trehalose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 827026-06-2
6,6'-dideoxy-6,6'-di(monobromoacetyl)amino-2,2',3,3',4,4'-hexa-O-benzyl-α-D-trehalose

: 111-68-2
1-Heptylamine

: 827026-07-3
6,6'-dideoxy-6,6'-di(monoheptaminoacetyl)amino-2,2',3,3',4,4'-hexa-O-benzyl-α-D-trehalose

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmc.2004.09.033

Reference yield:

: 125177-97-1,128188-35-2,74501-33-0
[(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl]-methanol

: 827026-07-3
6,6'-dideoxy-6,6'-di(monoheptaminoacetyl)amino-2,2',3,3',4,4'-hexa-O-benzyl-α-D-trehalose

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / CH₂Cl₂ / 0.5 h

2: 0.78 g / sodium azide / dimethylformamide / 12 h

3: 76 percent / trimethylphosphine; sodium hydroxide / tetrahydrofuran / 3 h / 50 °C

4: 74 percent / diisopropylcarbodiimide / dimethylformamide / 4 h / 20 °C

5: 75 percent / cesium carbonate / dimethylformamide / 20 °C

With pyridine; sodium hydroxide; sodium azide; caesium carbonate; diisopropyl-carbodiimide; trimethylphosphane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.09.033

Reference yield:

: 76790-47-1
6,6'-diazido-2,3,4,2',3',4'-hexa-O-benzyl-6,6'-dideoxy-α,α-trehalose

: 827026-07-3
6,6'-dideoxy-6,6'-di(monoheptaminoacetyl)amino-2,2',3,3',4,4'-hexa-O-benzyl-α-D-trehalose

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / trimethylphosphine; sodium hydroxide / tetrahydrofuran / 3 h / 50 °C

2: 74 percent / diisopropylcarbodiimide / dimethylformamide / 4 h / 20 °C

3: 75 percent / cesium carbonate / dimethylformamide / 20 °C

With sodium hydroxide; caesium carbonate; diisopropyl-carbodiimide; trimethylphosphane; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.09.033