2-(3-Buten-1-yloxy)-1-iodo-4-nitrobenzene

Base Information

Chemical Name:2-(3-Buten-1-yloxy)-1-iodo-4-nitrobenzene
CAS No.:107616-57-9
Molecular Formula:C₁₀H₁₀INO₃
Molecular Weight:319.099
Hs Code.:
DSSTox Substance ID:DTXSID101270936

Synonyms:2-(3-Buten-1-yloxy)-1-iodo-4-nitrobenzene;DTXSID101270936;107616-57-9

Suppliers and Price of 2-(3-Buten-1-yloxy)-1-iodo-4-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3-Buten-1-yloxy)-1-iodo-4-nitrobenzene

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:318.97054
Heavy Atom Count:15
Complexity:229

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CCCOC1=C(C=CC(=C1)[N+](=O)[O-])I

Technology Process of 2-(3-Buten-1-yloxy)-1-iodo-4-nitrobenzene

There total 3 articles about 2-(3-Buten-1-yloxy)-1-iodo-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 2-(3-butenyloxy)-4-nitrobenzenediazonium tetrafluoroborate

: 107616-57-9
2-(but-3-enyloxy)-1-iodo-4-nitrobenzene

: 107616-58-0
4-(iodomethyl)-7-nitrochroman

Guidance literature:: With sodium iodide; In acetone; for 0.25h;
DOI:10.1021/jo00386a007

Reference yield:

: 107616-21-7
2-(3-butenyloxy)-4-nitroaniline

: 107616-57-9
2-(but-3-enyloxy)-1-iodo-4-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / amyl nitrite, fluoroboric acid / ethanol; diethyl ether

2: 8 percent / NaI / acetone / 0.25 h

With tetrafluoroboric acid; n-Amyl nitrite; sodium iodide; In diethyl ether; ethanol; acetone;
DOI:10.1021/jo00386a007