2-(2-methylcyclohex-1-enecarbonyl)-3-(2,4,6-trimethoxyphenyl)acrylic acid methyl ester

Base Information

• Chemical Name: 2-(2-methylcyclohex-1-enecarbonyl)-3-(2,4,6-trimethoxyphenyl)acrylic acid methyl ester
• CAS No.: 638186-73-9
• Molecular Formula: C₂₁H₂₆O₆
• Molecular Weight: 374.434
• Mol file: 638186-73-9.mol

Synonyms:2-(2-methylcyclohex-1-enecarbonyl)-3-(2,4,6-trimethoxyphenyl)acrylic acid methyl ester

Chemical Property of 2-(2-methylcyclohex-1-enecarbonyl)-3-(2,4,6-trimethoxyphenyl)acrylic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 2-(2-methylcyclohex-1-enecarbonyl)-3-(2,4,6-trimethoxyphenyl)acrylic acid methyl ester

There total 1 articles about 2-(2-methylcyclohex-1-enecarbonyl)-3-(2,4,6-trimethoxyphenyl)acrylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4,6-trimethoxybenzaldehyde (830-79-5) + 3-(2-methyl-cyclohex-1-enyl)-3-oxo-propionic acid methyl ester → 2-(2-methylcyclohex-1-enecarbonyl)-3-(2,4,6-trimethoxyphenyl)acrylic acid methyl ester (638186-73-9)

Guidance literature:

With piperidine; acetic acid; In benzene; Heating;

DOI:10.1021/ja037910b

Reference yield: 95.0%

2-(2-methylcyclohex-1-enecarbonyl)-3-(2,4,6-trimethoxyphenyl)acrylic acid methyl ester (638186-73-9) → methyl 3a-methyl-1-oxo-3-(2,4,6-trimethoxyphenyl)-2,3,3a,4,5,6-hexahydro-1H-indene-2-carboxylate ester

Guidance literature:

copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 25 ℃; for 4h;

DOI:10.1021/ja077162g

Reference yield: 95.0%

2-(2-methylcyclohex-1-enecarbonyl)-3-(2,4,6-trimethoxyphenyl)acrylic acid methyl ester (638186-73-9) → 3a-methyl1-oxo-3-(2,4,6-trimethoxyphenyl)-2,3,3a,4,5,6-hexahydro-1H-indene-2-carboxylic acid methyl ester

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); In 1,2-dichloro-ethane; at 25 ℃; for 4h;

DOI:10.1021/ja037910b

upstream raw materials:

2,4,6-trimethoxybenzaldehyde