3-(2-[1,3]dioxan-2-yl-6-methoxymethoxy-phenyl)-6,7-dihydro-5H-benzo[d]isoxazol-4-one

Base Information

• Chemical Name: 3-(2-[1,3]dioxan-2-yl-6-methoxymethoxy-phenyl)-6,7-dihydro-5H-benzo[d]isoxazol-4-one
• CAS No.: 577975-53-2
• Molecular Formula: C₁₉H₂₁NO₆
• Molecular Weight: 359.379

Synonyms:3-(2-[1,3]dioxan-2-yl-6-methoxymethoxy-phenyl)-6,7-dihydro-5H-benzo[d]isoxazol-4-one

Chemical Property of 3-(2-[1,3]dioxan-2-yl-6-methoxymethoxy-phenyl)-6,7-dihydro-5H-benzo[d]isoxazol-4-one

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(2-[1,3]dioxan-2-yl-6-methoxymethoxy-phenyl)-6,7-dihydro-5H-benzo[d]isoxazol-4-one

There total 3 articles about 3-(2-[1,3]dioxan-2-yl-6-methoxymethoxy-phenyl)-6,7-dihydro-5H-benzo[d]isoxazol-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

1,3-cylohexanedione (504-02-9) + 2-[1,3]dioxan-2-yl-6-methoxymethoxy-benzonitrile N-oxide (579488-91-8) → 3-(2-[1,3]dioxan-2-yl-6-methoxymethoxy-phenyl)-6,7-dihydro-5H-benzo[d]isoxazol-4-one (577975-53-2)

Guidance literature:

With 4 A molecular sieve; In isopropyl alcohol; at 50 ℃; for 36h;

DOI:10.1055/s-2003-41436

Reference yield: 76.0%

→ 3-(2-[1,3]dioxan-2-yl-6-methoxymethoxy-phenyl)-6,7-dihydro-5H-benzo[d]isoxazol-4-one (577975-53-2)

Guidance literature:

Reference yield:

2-[1,3]dioxan-2-yl-6-methoxymethoxy-benzaldehyde oxime → 3-(2-[1,3]dioxan-2-yl-6-methoxymethoxy-phenyl)-6,7-dihydro-5H-benzo[d]isoxazol-4-one (577975-53-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / N-chlorosuccinimide (NCS); NEt₃ / CH₂Cl₂ / 20 °C

2: 76 percent / NEt₃ / ethanol / 24 h / 50 °C

With N-chloro-succinimide; triethylamine; In ethanol; dichloromethane;

DOI:10.1016/S0040-4039(03)00614-2

upstream raw materials:

1,3-cylohexanedione

2-[1,3]dioxan-2-yl-6-methoxymethoxy-benzonitrile N-oxide

Downstream raw materials:

1,8-dihydroxy-9,10-anthracenedione

C₂₃H₂₁NO₄

C₂₁H₁₉NO₄

C₂₁H₁₇NO₄

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