C₅₉H₈₂N₁₀O₁₂

Base Information

Chemical Name:C₅₉H₈₂N₁₀O₁₂
CAS No.:1316857-63-2
Molecular Formula:C₅₉H₈₂N₁₀O₁₂
Molecular Weight:1123.36
Hs Code.:

C<sub>59</sub>H<sub>82</sub>N<sub>10</sub>O<sub>12</sub>

Synonyms:C₅₉H₈₂N₁₀O₁₂

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Chemical Property of C₅₉H₈₂N₁₀O₁₂

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Technology Process of C₅₉H₈₂N₁₀O₁₂

There total 12 articles about C₅₉H₈₂N₁₀O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1316857-62-1
C₆₂H₉₀N₁₀O₁₂Si

: 1316857-63-2
C₅₉H₈₂N₁₀O₁₂

Guidance literature:: With cesium fluoride; In acetonitrile; at 25 ℃; for 14h;
DOI:10.1039/c1ob05606a

Reference yield:

: C₃₆H₅₅IN₆O₈

: 1316857-63-2
C₅₉H₈₂N₁₀O₁₂

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 4 h / 25 °C

2: sodium azide / N,N-dimethyl-formamide / 72 h / 110 °C

3: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 70 °C

4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 12 h / 25 °C

5: cesium fluoride / acetonitrile / 14 h / 25 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium azide; triethylamine; N-ethyl-N,N-diisopropylamine; cesium fluoride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 3: Huisgen-Sharpless 1,3-dipolar cycloaddition / 4: Sonogashira coupling;
DOI:10.1039/c1ob05606a

Reference yield:

: 1316857-59-6
C₁₄H₁₇IO₄

: 1316857-63-2
C₅₉H₈₂N₁₀O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride; methanol / 4 h / 50 °C

2: sodium hydroxide / water; dimethyl sulfoxide / 18 h / 25 °C

3: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C

4: triethylamine / dichloromethane / 4 h / 25 °C

5: sodium azide / N,N-dimethyl-formamide / 72 h / 110 °C

6: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 70 °C

7: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 12 h / 25 °C

8: cesium fluoride / acetonitrile / 14 h / 25 °C

With hydrogenchloride; methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium azide; triethylamine; N-ethyl-N,N-diisopropylamine; cesium fluoride; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; 3: Huisgen-Sharpless 1,3-dipolar cycloaddition / 6: Huisgen-Sharpless 1,3-dipolar cycloaddition / 7: Sonogashira coupling;
DOI:10.1039/c1ob05606a