1-Deuterio-cis-2,3-diphenyl-trans-1-benzolsulfonyl-cyclopropan

Base Information

• Chemical Name: 1-Deuterio-cis-2,3-diphenyl-trans-1-benzolsulfonyl-cyclopropan
• CAS No.: 71606-32-1
• Molecular Formula: C₂₁H₁₈O₂S
• Molecular Weight: 335.431
• Mol file: 71606-32-1.mol

Synonyms:1-Deuterio-cis-2,3-diphenyl-trans-1-benzolsulfonyl-cyclopropan

Chemical Property of 1-Deuterio-cis-2,3-diphenyl-trans-1-benzolsulfonyl-cyclopropan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1-Deuterio-cis-2,3-diphenyl-trans-1-benzolsulfonyl-cyclopropan

There total 5 articles about 1-Deuterio-cis-2,3-diphenyl-trans-1-benzolsulfonyl-cyclopropan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-Diphenyl-3-benzolsulfonyl-cyclopropen (17637-56-8) → 1-Deuterio-cis-2,3-diphenyl-trans-1-benzolsulfonyl-cyclopropan (71606-32-1)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / Pd-C

2: KOEt, EtOD

With ethyl [2]alcohol; potassium ethoxide; hydrogen; palladium on activated charcoal;

DOI:10.1021/ja00993a023

Reference yield:

sodium benzenesulfonate (873-55-2) → 1-Deuterio-cis-2,3-diphenyl-trans-1-benzolsulfonyl-cyclopropan (71606-32-1)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) HBF₄, (ii) /BRN= 3598406/

2: H₂ / Pd-C

3: KOEt, EtOD

With ethyl [2]alcohol; potassium ethoxide; hydrogen; palladium on activated charcoal;

DOI:10.1021/ja00993a023

Reference yield:

(cyclopropylsulfonyl)benzene (17637-57-9) → 1-Deuterio-cis-2,3-diphenyl-trans-1-benzolsulfonyl-cyclopropan (71606-32-1)

Guidance literature:

With ethyl [2]alcohol; potassium ethoxide; In diethylene glycol dimethyl ether; at 20 ℃; Rate constant; other reaction partners;

DOI:10.1021/ja00993a023

upstream raw materials:

(cyclopropylsulfonyl)benzene

cis-2,3-Diphenyl-trans-1-benzolsulfonyl-cyclopropan

cis-2,3-Diphenyl-cis-1-benzolsulfonyl-cyclopropan

1,2-Diphenyl-3-benzolsulfonyl-cyclopropen