C₂₁H₂₄O₁₃

Base Information

Chemical Name:C₂₁H₂₄O₁₃
CAS No.:1427054-89-4
Molecular Formula:C₂₁H₂₄O₁₃
Molecular Weight:484.414
Hs Code.:

C<sub>21</sub>H<sub>24</sub>O<sub>13</sub>

Synonyms:C₂₁H₂₄O₁₃

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Chemical Property of C₂₁H₂₄O₁₃

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Technology Process of C₂₁H₂₄O₁₃

There total 4 articles about C₂₁H₂₄O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1427054-86-1
C₅₆H₅₄O₁₃

: 1427054-89-4
C₂₁H₂₄O₁₃

Guidance literature:: With hydrogen; palladium(II) hydroxide; In ethyl acetate; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c3ob00046j

Reference yield:

: 1427054-81-6
C₂₂H₂₀O₈

: 1427054-89-4
C₂₁H₂₄O₁₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

1.2: 12 h / 0 °C / Inert atmosphere

2.1: hydrogen; palladium(II) hydroxide / ethyl acetate / 12 h / 20 °C / Inert atmosphere

With hydrogen; palladium(II) hydroxide; In dichloromethane; ethyl acetate;
DOI:10.1039/c3ob00046j

Reference yield:

: C₂₂H₂₂O₈

: 1427054-89-4
C₂₁H₂₄O₁₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-iodo-succinimide; tetra-(n-butyl)ammonium iodide / dichloromethane / 5 h / 50 °C / Inert atmosphere

2.1: dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

2.2: 12 h / 0 °C / Inert atmosphere

3.1: hydrogen; palladium(II) hydroxide / ethyl acetate / 12 h / 20 °C / Inert atmosphere

With N-iodo-succinimide; hydrogen; palladium(II) hydroxide; tetra-(n-butyl)ammonium iodide; In dichloromethane; ethyl acetate;
DOI:10.1039/c3ob00046j