2,3-di-O-benzoyl-4,6-O-(1-methoxycarbonylethylidene)-D-glucopyranosyl trichloroacetimidate

Base Information

Chemical Name:2,3-di-O-benzoyl-4,6-O-(1-methoxycarbonylethylidene)-D-glucopyranosyl trichloroacetimidate
CAS No.:143394-76-7
Molecular Formula:C₂₆H₂₄Cl₃NO₁₀
Molecular Weight:616.836
Hs Code.:

Synonyms:2,3-di-O-benzoyl-4,6-O-(1-methoxycarbonylethylidene)-D-glucopyranosyl trichloroacetimidate

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Chemical Property of 2,3-di-O-benzoyl-4,6-O-(1-methoxycarbonylethylidene)-D-glucopyranosyl trichloroacetimidate

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Technology Process of 2,3-di-O-benzoyl-4,6-O-(1-methoxycarbonylethylidene)-D-glucopyranosyl trichloroacetimidate

There total 5 articles about 2,3-di-O-benzoyl-4,6-O-(1-methoxycarbonylethylidene)-D-glucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 138857-87-1,138857-88-2
2,3-di-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-D-glucopyranose

: 545-06-2
trichloroacetonitrile

: 143394-76-7
2,3-di-O-benzoyl-4,6-O-(1-methoxycarbonylethylidene)-D-glucopyranosyl trichloroacetimidate

Guidance literature:: With potassium carbonate; In dichloromethane; for 24h; Ambient temperature;

Reference yield:

: 65725-42-0,65725-43-1,138857-51-9
benzyl 2,3-di-O-benzoyl-D-glucopyranoside

: 143394-76-7
2,3-di-O-benzoyl-4,6-O-(1-methoxycarbonylethylidene)-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 4 steps

1: 29 percent / NOBF₄ / CH₂Cl₂ / 5 h / -20 °C

2: TMSOTf / CH₂Cl₂ / 20 h / Ambient temperature

3: 100 percent / H₂ / 10percent Pd/C / acetic acid / 24 h / 760 Torr

4: 86 percent / K₂CO₃ / CH₂Cl₂ / 24 h / Ambient temperature

With hydrogen; potassium carbonate; nitrosonium tetrafluoroborate; palladium on activated charcoal; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; acetic acid;

Reference yield:

: 138857-57-5,138857-63-3,138857-94-0
C₃₃H₄₂O₈Si₂

: 143394-76-7
2,3-di-O-benzoyl-4,6-O-(1-methoxycarbonylethylidene)-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / TMSOTf / CH₂Cl₂ / 1.) 0 deg C, 2.) room temperature, 24 h

2: 100 percent / H₂ / 10percent Pd/C / acetic acid / 24 h / 760 Torr

3: 86 percent / K₂CO₃ / CH₂Cl₂ / 24 h / Ambient temperature

With hydrogen; potassium carbonate; palladium on activated charcoal; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; acetic acid;