1-(1-(4-tert-butylbenzyl)-5-oxo-4-propyl-4,5-dihydro-1H-1,2,4-triazol-3-yl)-2,2,2-trifluoroethyl 4-(1-tert-butoxy-2-methyl-1-oxopropan-2-ylthio)benzoate

Base Information

• Chemical Name: 1-(1-(4-tert-butylbenzyl)-5-oxo-4-propyl-4,5-dihydro-1H-1,2,4-triazol-3-yl)-2,2,2-trifluoroethyl 4-(1-tert-butoxy-2-methyl-1-oxopropan-2-ylthio)benzoate
• CAS No.: 1232163-56-2
• Molecular Formula: C₃₃H₄₂F₃N₃O₅S
• Molecular Weight: 649.775

Synonyms:1-(1-(4-tert-butylbenzyl)-5-oxo-4-propyl-4,5-dihydro-1H-1,2,4-triazol-3-yl)-2,2,2-trifluoroethyl 4-(1-tert-butoxy-2-methyl-1-oxopropan-2-ylthio)benzoate

Chemical Property of 1-(1-(4-tert-butylbenzyl)-5-oxo-4-propyl-4,5-dihydro-1H-1,2,4-triazol-3-yl)-2,2,2-trifluoroethyl 4-(1-tert-butoxy-2-methyl-1-oxopropan-2-ylthio)benzoate

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Technology Process of 1-(1-(4-tert-butylbenzyl)-5-oxo-4-propyl-4,5-dihydro-1H-1,2,4-triazol-3-yl)-2,2,2-trifluoroethyl 4-(1-tert-butoxy-2-methyl-1-oxopropan-2-ylthio)benzoate

There total 1 articles about 1-(1-(4-tert-butylbenzyl)-5-oxo-4-propyl-4,5-dihydro-1H-1,2,4-triazol-3-yl)-2,2,2-trifluoroethyl 4-(1-tert-butoxy-2-methyl-1-oxopropan-2-ylthio)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.5%

4-(1-tert-butoxy-2-methyl-1-oxopropan-2-ylthio)benzoic acid (521084-52-6) + 1-(4-tert-butylbenzyl)-4-propyl-3-(2,2,2-trifluoro-1-hydroxyethyl)-1H-1,2,4-triazol-5(4H)-one (1232163-53-9) → 1-(1-(4-tert-butylbenzyl)-5-oxo-4-propyl-4,5-dihydro-1H-1,2,4-triazol-3-yl)-2,2,2-trifluoroethyl 4-(1-tert-butoxy-2-methyl-1-oxopropan-2-ylthio)benzoate (1232163-56-2)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield: 80.8%

1-(1-(4-tert-butylbenzyl)-5-oxo-4-propyl-4,5-dihydro-1H-1,2,4-triazol-3-yl)-2,2,2-trifluoroethyl 4-(1-tert-butoxy-2-methyl-1-oxopropan-2-ylthio)benzoate (1232163-56-2) → 2-(4-((1-(1-(4-tert-butylbenzyl)-5-oxo-4-propyl-4,5-dihydro-1H-1,2,4-triazol-3-yl)-2,2,2-trifluoroethoxy)carbonyl)phenylthio)-2-methylpropanoic acid (1232163-50-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 16h;

upstream raw materials:

4-(1-tert-butoxy-2-methyl-1-oxopropan-2-ylthio)benzoic acid

1-(4-tert-butylbenzyl)-4-propyl-3-(2,2,2-trifluoro-1-hydroxyethyl)-1H-1,2,4-triazol-5(4H)-one

Downstream raw materials:

2-(4-((1-(1-(4-tert-butylbenzyl)-5-oxo-4-propyl-4,5-dihydro-1H-1,2,4-triazol-3-yl)-2,2,2-trifluoroethoxy)carbonyl)phenylthio)-2-methylpropanoic acid

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