C₂₃H₃₂BrNO

Base Information

• Chemical Name: C₂₃H₃₂BrNO
• CAS No.: 1010685-26-3
• Molecular Formula: C₂₃H₃₂BrNO
• Molecular Weight: 418.417
• Mol file: 1010685-26-3.mol

Synonyms:C₂₃H₃₂BrNO

Chemical Property of C₂₃H₃₂BrNO

Chemical Property:

Purity/Quality:

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Technology Process of C₂₃H₃₂BrNO

There total 1 articles about C₂₃H₃₂BrNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2-iodo-5-bromopyridine (223463-13-6) + 4-dodecyloxybenzene boronic acid (169760-27-4) → C23H32BrNO (1010685-26-3)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; at 100 ℃; for 24h; Inert atmosphere;

DOI:10.1039/b714291a

Reference yield: 99.0%

1-dodecyne (765-03-7) + C23H32BrNO (1010685-26-3) → C35H53NO (1010685-27-4)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 100 ℃; for 36h; Inert atmosphere;

DOI:10.1039/b714291a

upstream raw materials:

2-iodo-5-bromopyridine

4-dodecyloxybenzene boronic acid

Downstream raw materials:

C₃₅H₅₃NO