4-(5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethoxy)nitrobenzene

Base Information

Chemical Name:4-(5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethoxy)nitrobenzene
CAS No.:224954-02-3
Molecular Formula:C₂₇H₂₉NO₅
Molecular Weight:447.531
Hs Code.:

Synonyms:4-(5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethoxy)nitrobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethoxy)nitrobenzene

Chemical Property:

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Technology Process of 4-(5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethoxy)nitrobenzene

There total 1 articles about 4-(5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethoxy)nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 183142-41-8
5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-carbinol

: 224954-02-3
4-(5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethoxy)nitrobenzene

Guidance literature:: With sodium hydride; Yield given; Multistep reaction; 1.) DMF, 25 deg C, 1 h, 2.) DMF, 25 deg C, 3 h;
DOI:10.1021/jm980549x

Reference yield: 75.0%

: 224954-02-3
4-(5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethoxy)nitrobenzene

: 224954-03-4
4-(5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethoxy)aniline

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 48h; under 3102.89 Torr; Ambient temperature;
DOI:10.1021/jm980549x

Reference yield:

: 224954-02-3
4-(5-benzyloxy-2,2,4,6,7-pentamethyl-1-benzofuran-3-ylmethoxy)nitrobenzene

: 5-<4-(2,3-dihydro-5-hydroxy-2,2,4,6,7-pentamethylbenzofuran-3-ylmethoxy)phenylmethyl>thiazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / H₂ / 10 percent Pd/C / ethyl acetate / 48 h / 3102.89 Torr / Ambient temperature

2: 1.) NaNO₂, aq. HBr, 2.) Cu₂O / 1.) methanol, acetone, 5 deg C, 30 min, 2.) methanol, acetone, 38 deg C

3: sodium acetate / ethanol / 12 h / Heating

4: 73 percent / 2N aq. HCl / ethanol / 12 h / Heating

5: 54 percent / conc. aq. HCl / acetic acid / 2 h / 90 °C

With copper(I) oxide; hydrogenchloride; hydrogen bromide; hydrogen; sodium acetate; sodium nitrite; palladium on activated charcoal; In ethanol; acetic acid; ethyl acetate;
DOI:10.1021/jm980549x