3β, 16β,26-trihydroxycholest-5-en-22-one 16-O-(2-O-4-methoxybenzoyl-β-D-xylopyranosyl)-(1->3)-2-O-acetyl-α-L-arabinopyranoside

Base Information

Chemical Name:3β, 16β,26-trihydroxycholest-5-en-22-one 16-O-(2-O-4-methoxybenzoyl-β-D-xylopyranosyl)-(1->3)-2-O-acetyl-α-L-arabinopyranoside
CAS No.:1253283-77-0
Molecular Formula:C₄₇H₆₈O₁₅
Molecular Weight:873.048
Hs Code.:

Synonyms:3β, 16β,26-trihydroxycholest-5-en-22-one 16-O-(2-O-4-methoxybenzoyl-β-D-xylopyranosyl)-(1->3)-2-O-acetyl-α-L-arabinopyranoside

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Chemical Property of 3β, 16β,26-trihydroxycholest-5-en-22-one 16-O-(2-O-4-methoxybenzoyl-β-D-xylopyranosyl)-(1->3)-2-O-acetyl-α-L-arabinopyranoside

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Technology Process of 3β, 16β,26-trihydroxycholest-5-en-22-one 16-O-(2-O-4-methoxybenzoyl-β-D-xylopyranosyl)-(1->3)-2-O-acetyl-α-L-arabinopyranoside

There total 2 articles about 3β, 16β,26-trihydroxycholest-5-en-22-one 16-O-(2-O-4-methoxybenzoyl-β-D-xylopyranosyl)-(1->3)-2-O-acetyl-α-L-arabinopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1253283-92-9
C₈₁H₁₂₆O₁₇Si₃

: 1253283-77-0
3β, 16β,26-trihydroxycholest-5-en-22-one 16-O-(2-O-4-methoxybenzoyl-β-D-xylopyranosyl)-(1->3)-2-O-acetyl-α-L-arabinopyranoside

Guidance literature:: C₈₁H₁₂₆O₁₇Si₃; With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 20 ℃; for 5h;

With dichloro bis(acetonitrile) palladium(II); In water; acetone; at 20 ℃; for 3h;
DOI:10.1016/j.bmcl.2010.07.085

Reference yield: 62.0%

: C₇₇H₁₃₈O₁₅Si₅

: 1253283-77-0
3β, 16β,26-trihydroxycholest-5-en-22-one 16-O-(2-O-4-methoxybenzoyl-β-D-xylopyranosyl)-(1->3)-2-O-acetyl-α-L-arabinopyranoside

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); In dichloromethane; water; acetone; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2016.05.049