<β-(benzylthio)-β,β-dimethylpropionyl>-Tyr(Me)-Phe-Gln-Asn-Cys(Bzl)-Pro-Arg(Tos)-Val-NH2

Base Information

• Chemical Name: <β-(benzylthio)-β,β-dimethylpropionyl>-Tyr(Me)-Phe-Gln-Asn-Cys(Bzl)-Pro-Arg(Tos)-Val-NH2
• CAS No.: 138093-26-2
• Molecular Formula: C₇₃H₉₆N₁₄O₁₄S₃
• Molecular Weight: 1489.85
• Mol file: 138093-26-2.mol

Synonyms:<β-(benzylthio)-β,β-dimethylpropionyl>-Tyr(Me)-Phe-Gln-Asn-Cys(Bzl)-Pro-Arg(Tos)-Val-NH2

Chemical Property of <β-(benzylthio)-β,β-dimethylpropionyl>-Tyr(Me)-Phe-Gln-Asn-Cys(Bzl)-Pro-Arg(Tos)-Val-NH2

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of <β-(benzylthio)-β,β-dimethylpropionyl>-Tyr(Me)-Phe-Gln-Asn-Cys(Bzl)-Pro-Arg(Tos)-Val-NH2

There total 1 articles about <β-(benzylthio)-β,β-dimethylpropionyl>-Tyr(Me)-Phe-Gln-Asn-Cys(Bzl)-Pro-Arg(Tos)-Val-NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.2%

L-valinamide (4540-60-7,20108-78-5) + <(β-benzylthio)-β,β-dimethylpropionyl>-Tyr(Me)-Phe-Gln-Asn-Cys(Bzl)-Pro-Arg(Tos) (138093-18-2) → <β-(benzylthio)-β,β-dimethylpropionyl>-Tyr(Me)-Phe-Gln-Asn-Cys(Bzl)-Pro-Arg(Tos)-Val-NH2 (138093-26-2)

Guidance literature:

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 6h; Ambient temperature;

DOI:10.1021/jm00080a027

Reference yield:

<β-(benzylthio)-β,β-dimethylpropionyl>-Tyr(Me)-Phe-Gln-Asn-Cys(Bzl)-Pro-Arg(Tos)-Val-NH2 (138093-26-2) → C52H76N14O12S2 (138093-15-9)

Guidance literature:

With ammonia; sodium; potassium hexacyanoferrate(III); Yield given. Multistep reaction; 1.) reflux, 30 s, 2.) water, 20 min;

DOI:10.1021/jm00080a027

upstream raw materials:

L-valinamide

<(β-benzylthio)-β,β-dimethylpropionyl>-Tyr(Me)-Phe-Gln-Asn-Cys(Bzl)-Pro-Arg(Tos)

Downstream raw materials:

C₅₂H₇₆N₁₄O₁₂S₂