(2R,4R,5S)-5-(2-cyanoethyl)-4-(4-methoxybenzyloxy)-2-methyl-2-propyloxolane

Base Information

Chemical Name:(2R,4R,5S)-5-(2-cyanoethyl)-4-(4-methoxybenzyloxy)-2-methyl-2-propyloxolane
CAS No.:1078738-11-0
Molecular Formula:C₁₉H₂₇NO₃
Molecular Weight:317.428
Hs Code.:

Synonyms:(2R,4R,5S)-5-(2-cyanoethyl)-4-(4-methoxybenzyloxy)-2-methyl-2-propyloxolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,4R,5S)-5-(2-cyanoethyl)-4-(4-methoxybenzyloxy)-2-methyl-2-propyloxolane

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Technology Process of (2R,4R,5S)-5-(2-cyanoethyl)-4-(4-methoxybenzyloxy)-2-methyl-2-propyloxolane

There total 1 articles about (2R,4R,5S)-5-(2-cyanoethyl)-4-(4-methoxybenzyloxy)-2-methyl-2-propyloxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 935761-66-3
3-[(2S,3R,5R)-3-hydroxy-5-methyl-5-propyloxolan-2-yl]propanenitrile

: 824-94-2
p-methoxybenzyl chloride

: 1078738-11-0
(2R,4R,5S)-5-(2-cyanoethyl)-4-(4-methoxybenzyloxy)-2-methyl-2-propyloxolane

Guidance literature:: 3-[(2S,3R,5R)-3-hydroxy-5-methyl-5-propyloxolan-2-yl]propanenitrile; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.0833333h; Inert atmosphere;

p-methoxybenzyl chloride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;
DOI:10.1021/ol8021676

Reference yield: 86.0%

: 1078738-11-0
(2R,4R,5S)-5-(2-cyanoethyl)-4-(4-methoxybenzyloxy)-2-methyl-2-propyloxolane

: 1078737-98-0
(2R,4R,5S)-5-(2-formylethyl)-4-(4-methoxybenzyloxy)-2-methyl-2-propyloxolane

Guidance literature:: (2R,4R,5S)-5-(2-cyanoethyl)-4-(4-methoxybenzyloxy)-2-methyl-2-propyloxolane; With diisobutylaluminium hydride; In hexane; toluene; at -78 ℃; for 1h; Inert atmosphere;

With water; Rochelle's salt; In hexane; toluene; at 20 ℃; for 0.166667h;
DOI:10.1021/ol8021676