C₂₇H₃₇ClO₄S

Base Information

Chemical Name:C₂₇H₃₇ClO₄S
CAS No.:74726-85-5
Molecular Formula:C₂₇H₃₇ClO₄S
Molecular Weight:493.107
Hs Code.:

C<sub>27</sub>H<sub>37</sub>ClO<sub>4</sub>S

Synonyms:C₂₇H₃₇ClO₄S

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Chemical Property of C₂₇H₃₇ClO₄S

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Technology Process of C₂₇H₃₇ClO₄S

There total 6 articles about C₂₇H₃₇ClO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 74726-78-6
1-iodo-2-phenylthiomethyl-4,6-dimethoxy-benzene

: 74726-80-0
C₁₁H₂₃ClO

: 74726-85-5
C₂₇H₃₇ClO₄S

Guidance literature:: With triethylamine; palladium dichloride; In benzene; at 120 ℃; for 20h; under 9120 Torr;
DOI:10.1246/cl.1980.369

Reference yield:

: 19491-18-0
methyl 2-bromo-3,5-dimethoxybenzoate

: 74726-85-5
C₂₇H₃₇ClO₄S

Guidance literature:: Multi-step reaction with 5 steps

1: 52 percent / lithium aluminium hydride / diethyl ether / 0 °C

2: 1.) n-BuLi, 2.) iodine / 1.) THF, -78 deg C, 2.) -40 deg C

3: SOCl₂

4: sodium ethoxide

5: 72 percent / NEt₃ / PdCl₂ / benzene / 20 h / 120 °C / 9120 Torr

With lithium aluminium tetrahydride; n-butyllithium; thionyl chloride; iodine; sodium ethanolate; triethylamine; palladium dichloride; In diethyl ether; benzene;
DOI:10.1246/cl.1980.369

Reference yield:

: 2150-37-0
methyl 3,5-dimethoxybenzoate

: 74726-85-5
C₂₇H₃₇ClO₄S

Guidance literature:: Multi-step reaction with 6 steps

1: bromine / CCl₄ / 6 h / Heating; Irradiation

2: 52 percent / lithium aluminium hydride / diethyl ether / 0 °C

3: 1.) n-BuLi, 2.) iodine / 1.) THF, -78 deg C, 2.) -40 deg C

4: SOCl₂

5: sodium ethoxide

6: 72 percent / NEt₃ / PdCl₂ / benzene / 20 h / 120 °C / 9120 Torr

With lithium aluminium tetrahydride; n-butyllithium; thionyl chloride; bromine; iodine; sodium ethanolate; triethylamine; palladium dichloride; In tetrachloromethane; diethyl ether; benzene;
DOI:10.1246/cl.1980.369