3-(2-(benzyloxy)-1-(2,3-dichlorophenyl)ethyl)-1-methyl-1-(1-methylpiperidine-4-yl)urea

Base Information

Chemical Name:3-(2-(benzyloxy)-1-(2,3-dichlorophenyl)ethyl)-1-methyl-1-(1-methylpiperidine-4-yl)urea
CAS No.:1394858-94-6
Molecular Formula:C₂₃H₂₉Cl₂N₃O₂
Molecular Weight:450.408
Hs Code.:

Synonyms:3-(2-(benzyloxy)-1-(2,3-dichlorophenyl)ethyl)-1-methyl-1-(1-methylpiperidine-4-yl)urea

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Chemical Property of 3-(2-(benzyloxy)-1-(2,3-dichlorophenyl)ethyl)-1-methyl-1-(1-methylpiperidine-4-yl)urea

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Technology Process of 3-(2-(benzyloxy)-1-(2,3-dichlorophenyl)ethyl)-1-methyl-1-(1-methylpiperidine-4-yl)urea

There total 7 articles about 3-(2-(benzyloxy)-1-(2,3-dichlorophenyl)ethyl)-1-methyl-1-(1-methylpiperidine-4-yl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 73579-08-5
Methyl-(1-methyl-[4]piperidyl)-amin

: 1394860-44-6
C₁₅H₁₅Cl₂NO

: 1394858-94-6
3-(2-(benzyloxy)-1-(2,3-dichlorophenyl)ethyl)-1-methyl-1-(1-methylpiperidine-4-yl)urea

Guidance literature:: C₁₅H₁₅Cl₂NO; With bis(trichloromethyl) carbonate; triethylamine; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

Methyl-(1-methyl-[4]piperidyl)-amin; In dichloromethane; at 20 ℃; for 1h;

Reference yield: 84.0%

: 73579-08-5
Methyl-(1-methyl-[4]piperidyl)-amin

: 32315-10-9
bis(trichloromethyl) carbonate

: 1394860-44-6
C₁₅H₁₅Cl₂NO

: 1394858-94-6
3-(2-(benzyloxy)-1-(2,3-dichlorophenyl)ethyl)-1-methyl-1-(1-methylpiperidine-4-yl)urea

Guidance literature:: bis(trichloromethyl) carbonate; C₁₅H₁₅Cl₂NO; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

Methyl-(1-methyl-[4]piperidyl)-amin; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 343787-47-3
2-bromo-1-(2,3-dichlorophenyl)ethanone

: 1394858-94-6
3-(2-(benzyloxy)-1-(2,3-dichlorophenyl)ethyl)-1-methyl-1-(1-methylpiperidine-4-yl)urea

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate; methanol / 1.5 h / 20 °C

2.1: potassium hydroxide / water; tetrahydrofuran / 20 °C

3.1: sodium / 20 - 70 °C / Inert atmosphere

4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C / Inert atmosphere

5.1: hydrazine hydrate / methanol / 2 h / Reflux

6.1: dichloromethane / 0.17 h / 20 °C / Inert atmosphere

6.2: 1 h / 20 °C

With methanol; sodium tetrahydroborate; di-isopropyl azodicarboxylate; sodium; hydrazine hydrate; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;