4-((4-methoxy-2,3,6-trimethylphenylsulfonyl)aminomethyl)benzylic alcohol

Base Information

Chemical Name:4-((4-methoxy-2,3,6-trimethylphenylsulfonyl)aminomethyl)benzylic alcohol
CAS No.:1414916-39-4
Molecular Formula:C₁₈H₂₃NO₄S
Molecular Weight:349.451
Hs Code.:

Synonyms:4-((4-methoxy-2,3,6-trimethylphenylsulfonyl)aminomethyl)benzylic alcohol

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Chemical Property of 4-((4-methoxy-2,3,6-trimethylphenylsulfonyl)aminomethyl)benzylic alcohol

Chemical Property:

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Technology Process of 4-((4-methoxy-2,3,6-trimethylphenylsulfonyl)aminomethyl)benzylic alcohol

There total 2 articles about 4-((4-methoxy-2,3,6-trimethylphenylsulfonyl)aminomethyl)benzylic alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39895-56-2
4-hydroxymethyl-benzylamine

: 80745-07-9
4-methoxy-2,3,6-trimethylbenzenesulfonyl chloride

: 1414916-39-4
4-((4-methoxy-2,3,6-trimethylphenylsulfonyl)aminomethyl)benzylic alcohol

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; for 6.5h; Inert atmosphere;
DOI:10.1021/jm301058f

Reference yield:

: 56-91-7
p-aminomethylbenzoic acid

: 1414916-39-4
4-((4-methoxy-2,3,6-trimethylphenylsulfonyl)aminomethyl)benzylic alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 6.5 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;
DOI:10.1021/jm301058f

Reference yield:

: 1414916-39-4
4-((4-methoxy-2,3,6-trimethylphenylsulfonyl)aminomethyl)benzylic alcohol

: C₂₇H₃₆N₆O₈S*C₃H₃F₃O

Guidance literature:: Multi-step reaction with 4 steps

1: manganese(IV) oxide / tetrahydrofuran / Inert atmosphere

2: sodium cyanoborohydride / methanol / 4 h / 20 °C / Inert atmosphere

3: dichloromethane / 20 °C

4: triethylsilane; trifluoroacetic acid / dichloromethane / 3 h / 20 °C

With triethylsilane; manganese(IV) oxide; sodium cyanoborohydride; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm301058f