(-)-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)-N-phenylmaleimide

Base Information

Chemical Name:(-)-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)-N-phenylmaleimide
CAS No.:132374-45-9
Molecular Formula:C₂₀H₂₃NO₃S
Molecular Weight:357.474
Hs Code.:

Synonyms:(-)-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)-N-phenylmaleimide

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Chemical Property of (-)-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)-N-phenylmaleimide

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Technology Process of (-)-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)-N-phenylmaleimide

There total 3 articles about (-)-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)-N-phenylmaleimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 132345-22-3,132374-43-7
α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)-N-phenylsuccinimide

: 132374-45-9
(-)-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)-N-phenylmaleimide

Guidance literature:: With N-chloro-succinimide; In tetrachloromethane; for 6h; Heating;
DOI:10.1021/jo00006a005

Reference yield:

: 941-69-5
N-phenyl-maleimide

: 132374-45-9
(-)-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)-N-phenylmaleimide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / CH₂Cl₂ / 25 °C

2: 92 percent / N-chlorosuccinimide / CCl₄ / Heating

With N-chloro-succinimide; triethylamine; In tetrachloromethane; dichloromethane;

Reference yield:

: 71242-58-5
(1S,2R,4R)-(-)-10-mercaptoisoboneol

: 132374-45-9
(-)-α-(<(1S,2R,4R)-2-hydroxy-7,7-dimethylbicyclo<2.2.1>heptan-1-yl>methylthio)-N-phenylmaleimide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / CH₂Cl₂ / 25 °C

2: 92 percent / N-chlorosuccinimide / CCl₄ / Heating

With N-chloro-succinimide; triethylamine; In tetrachloromethane; dichloromethane;