methyl 2-O-benzoyl-4-deoxy-3-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-lyxo-hexopyranoside

Base Information

Chemical Name:methyl 2-O-benzoyl-4-deoxy-3-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-lyxo-hexopyranoside
CAS No.:174089-90-8
Molecular Formula:C₄₈H₄₄O₁₅
Molecular Weight:860.868
Hs Code.:

Synonyms:methyl 2-O-benzoyl-4-deoxy-3-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-lyxo-hexopyranoside

Suppliers and Price of methyl 2-O-benzoyl-4-deoxy-3-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-lyxo-hexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of methyl 2-O-benzoyl-4-deoxy-3-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-lyxo-hexopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl 2-O-benzoyl-4-deoxy-3-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-lyxo-hexopyranoside

There total 5 articles about methyl 2-O-benzoyl-4-deoxy-3-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₅H₄₉IO₁₅

: 174089-90-8
methyl 2-O-benzoyl-4-deoxy-3-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-lyxo-hexopyranoside

Guidance literature:: With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In ethyl acetate; under 3000.2 Torr; Yield given;
DOI:10.1016/0008-6215(95)00268-5

Reference yield:

: 14218-11-2,14218-30-5,61198-88-7,108438-33-1,108836-02-8,114682-36-9,127305-34-4,151377-77-4
2,3,4,6-Tetra-O-benzoyl-α-D-mannopyranosyl bromide

: 174089-90-8
methyl 2-O-benzoyl-4-deoxy-3-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / silver trifluoromethanesulfonate, 4 Angstroem molecular sieves / toluene; CH₂Cl₂ / 0.5 h / 0 °C

2: sodium cyanoborohydride / tetrahydrofuran / 0.33 h

3: triiodoimidazole, triphenylphosphine / toluene / 110 °C

4: H₂, aq. NaHCO₃ / Pd-C / ethyl acetate / 3000.2 Torr

With tri-iodoimidazole; 4 A molecular sieve; hydrogen; silver trifluoromethanesulfonate; sodium cyanoborohydride; sodium hydrogencarbonate; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene;
DOI:10.1016/0008-6215(95)00268-5

Reference yield:

: 91685-06-2
methyl 2-O-benzoyl-4, 6-O-benzylidene-α-D-mannopyranoside

: 174089-90-8
methyl 2-O-benzoyl-4-deoxy-3-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / silver trifluoromethanesulfonate, 4 Angstroem molecular sieves / toluene; CH₂Cl₂ / 0.5 h / 0 °C

2: sodium cyanoborohydride / tetrahydrofuran / 0.33 h

3: triiodoimidazole, triphenylphosphine / toluene / 110 °C

4: H₂, aq. NaHCO₃ / Pd-C / ethyl acetate / 3000.2 Torr

With tri-iodoimidazole; 4 A molecular sieve; hydrogen; silver trifluoromethanesulfonate; sodium cyanoborohydride; sodium hydrogencarbonate; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene;
DOI:10.1016/0008-6215(95)00268-5