C₅₅H₇₃NO₉

Base Information

• Chemical Name: C₅₅H₇₃NO₉
• CAS No.: 1354747-49-1
• Molecular Formula: C₅₅H₇₃NO₉
• Molecular Weight: 892.186
• Mol file: 1354747-49-1.mol

Synonyms:C₅₅H₇₃NO₉

Chemical Property of C₅₅H₇₃NO₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₅H₇₃NO₉

There total 20 articles about C₅₅H₇₃NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

C57H72Cl3NO10 → C48H69NO8 (1354747-50-4) + C55H73NO9 (1354747-49-1)

Guidance literature:

With water; potassium carbonate; In methanol; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol2032448

Reference yield:

C31H36O7 → C48H69NO8 (1354747-50-4) + C55H73NO9 (1354747-49-1)

Guidance literature:

Multi-step reaction with 5 steps

1: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; benzene / 0.67 h / 20 °C / Inert atmosphere

2: zinc / ethanol / 0.75 h / Inert atmosphere; Reflux

3: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / Inert atmosphere; Reflux

4: dichloromethane / 0.5 h / 20 °C / Inert atmosphere

5: water; potassium carbonate / methanol / 20 °C / Inert atmosphere

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; water; iodine; potassium carbonate; triphenylphosphine; zinc; In methanol; diethyl ether; ethanol; dichloromethane; benzene;

DOI:10.1021/ol2032448

Reference yield:

C31H35IO6 → C48H69NO8 (1354747-50-4) + C55H73NO9 (1354747-49-1)

Guidance literature:

Multi-step reaction with 4 steps

1: zinc / ethanol / 0.75 h / Inert atmosphere; Reflux

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / Inert atmosphere; Reflux

3: dichloromethane / 0.5 h / 20 °C / Inert atmosphere

4: water; potassium carbonate / methanol / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; water; potassium carbonate; zinc; In methanol; ethanol; dichloromethane;

DOI:10.1021/ol2032448

upstream raw materials:

1-deoxy-1-allyl-2,3,4,6-tetra-O-acetyl-D-galactopyranoside

C₃₁H₃₆O₅

C₃₃H₃₈O₇

C₃₁H₃₆O₆

Downstream raw materials:

C₅₆H₇₅NO₉

C₄₈H₆₇NO₇

C₇₃H₁₁₉NO₇

C₄₃H₇₄FNO₇