3-azidobenzyl 4-((4-amino-[1,1'-biphenyl]-3-yl)carbamoyl)benzylcarbamate

Base Information

Chemical Name:3-azidobenzyl 4-((4-amino-[1,1'-biphenyl]-3-yl)carbamoyl)benzylcarbamate
CAS No.:1393745-26-0
Molecular Formula:C₂₈H₂₄N₆O₃
Molecular Weight:492.537
Hs Code.:

Synonyms:3-azidobenzyl 4-((4-amino-[1,1'-biphenyl]-3-yl)carbamoyl)benzylcarbamate

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Chemical Property of 3-azidobenzyl 4-((4-amino-[1,1'-biphenyl]-3-yl)carbamoyl)benzylcarbamate

Chemical Property:

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Technology Process of 3-azidobenzyl 4-((4-amino-[1,1'-biphenyl]-3-yl)carbamoyl)benzylcarbamate

There total 3 articles about 3-azidobenzyl 4-((4-amino-[1,1'-biphenyl]-3-yl)carbamoyl)benzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₃₂N₆O₅

: 1393745-26-0
3-azidobenzyl 4-((4-amino-[1,1'-biphenyl]-3-yl)carbamoyl)benzylcarbamate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2012.06.017

Reference yield:

: 1393745-13-5
C₁₆H₁₄N₄O₄

: 1393745-26-0
3-azidobenzyl 4-((4-amino-[1,1'-biphenyl]-3-yl)carbamoyl)benzylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 78 °C

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.06.017