3β,6α-dihydroxy-5α-androstane

Base Information

• Chemical Name: 3β,6α-dihydroxy-5α-androstane
• CAS No.: 49643-13-2
• Molecular Formula: C₁₉H₃₂O₂
• Molecular Weight: 292.462
• Mol file: 49643-13-2.mol

Synonyms:3β,6α-dihydroxy-5α-androstane

Chemical Property of 3β,6α-dihydroxy-5α-androstane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3β,6α-dihydroxy-5α-androstane

There total 4 articles about 3β,6α-dihydroxy-5α-androstane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3β-acetoxyandrost-5-ene (13067-44-2) → 5α-androstan-3β-ol (1224-93-7,7657-50-3,7753-89-1,10085-14-0,15360-52-8,15360-53-9,36216-01-0,36216-02-1,1224-92-6) + 3β-acetoxy-5α-androstane (1236-13-1) + 3β,6α-dihydroxy-5α-androstane (49643-13-2) + 3β-acetoxy-6α-hydroxy-5α-androstane

Guidance literature:

With sodium hydroxide; borane; dihydrogen peroxide; Yield given; Multistep reaction. Further byproducts given. Yields of byproduct given; 1.) THF, 0 deg C, 4 h, 2.) THF, overnight;

Reference yield:

3β-acetoxyandrost-5-ene (13067-44-2) → 5α-androstan-3β-ol (1224-93-7,7657-50-3,7753-89-1,10085-14-0,15360-52-8,15360-53-9,36216-01-0,36216-02-1,1224-92-6) + 3β,6α-dihydroxy-5α-androstane (49643-13-2) + 3β,5α-dihydroxyandrostane (5223-92-7) + 3β-acetoxy-6α-hydroxy-5α-androstane

Guidance literature:

With sodium hydroxide; borane; dihydrogen peroxide; Yield given; Multistep reaction. Further byproducts given. Yields of byproduct given; 1.) THF, 0 deg C, 4 h, 2.) THF, overnight;

Reference yield:

3β-acetoxyandrost-5-ene (13067-44-2) → 5α-androstan-3β-ol (1224-93-7,7657-50-3,7753-89-1,10085-14-0,15360-52-8,15360-53-9,36216-01-0,36216-02-1,1224-92-6) + 3β,6α-dihydroxy-5α-androstane (49643-13-2) + 3β,6β-dihydroxy-5α-androstane + 3β-acetoxy-6α-hydroxy-5α-androstane

Guidance literature:

With sodium hydroxide; borane; dihydrogen peroxide; Yield given; Multistep reaction. Further byproducts given. Yields of byproduct given; 1.) THF, 0 deg C, 4 h, 2.) THF, overnight;

upstream raw materials:

3β-acetoxyandrost-5-ene

Refernces