2-2'-carbobenzyloxy-6'-methoxy-4'-methylphenyl-3,5-dichloro-1,4-hydroquinone

Base Information

Chemical Name:2-2'-carbobenzyloxy-6'-methoxy-4'-methylphenyl-3,5-dichloro-1,4-hydroquinone
CAS No.:125187-09-9
Molecular Formula:C₂₂H₁₈Cl₂O₅
Molecular Weight:433.288
Hs Code.:

Synonyms:2-2'-carbobenzyloxy-6'-methoxy-4'-methylphenyl-3,5-dichloro-1,4-hydroquinone

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Chemical Property of 2-2'-carbobenzyloxy-6'-methoxy-4'-methylphenyl-3,5-dichloro-1,4-hydroquinone

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Technology Process of 2-2'-carbobenzyloxy-6'-methoxy-4'-methylphenyl-3,5-dichloro-1,4-hydroquinone

There total 1 articles about 2-2'-carbobenzyloxy-6'-methoxy-4'-methylphenyl-3,5-dichloro-1,4-hydroquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 125187-08-8
2-(2,4-Dichloro-3,6-dioxo-cyclohexa-1,4-dienyl)-3-methoxy-5-methyl-benzoic acid methyl ester

: 100-51-6,185532-71-2
benzyl alcohol

: 125187-09-9
2-2'-carbobenzyloxy-6'-methoxy-4'-methylphenyl-3,5-dichloro-1,4-hydroquinone

Guidance literature:: With titanium(IV) isopropylate; at 120 - 130 ℃; for 16h;

Reference yield: 96.0%

: 125187-09-9
2-2'-carbobenzyloxy-6'-methoxy-4'-methylphenyl-3,5-dichloro-1,4-hydroquinone

: 125187-10-2
2-2'-carbobenzyloxy-6'-methoxy-4'-methylphenyl-3,5-dichloro-1,4-benzoquinone

Guidance literature:: With manganese(IV) oxide; In dichloromethane; for 0.166667h; Ambient temperature;

Reference yield:

: 125187-09-9
2-2'-carbobenzyloxy-6'-methoxy-4'-methylphenyl-3,5-dichloro-1,4-hydroquinone

: 125187-16-8
2-2'-carboxy-6'-methoxy-4'-methylphenyl-3-chloro-5-hydroxy-1,4-naphthoquinone

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / MnO₂ / CH₂Cl₂ / 0.17 h / Ambient temperature

2: 86 percent / ethyl acetate / 6 h / Ambient temperature

4: 1.) hydrogen, 2.) MnO₂ / 1.) Pd(OH)2 on carbon / 1.) ethyl acetate, 15 h, 50 psi, 2.) CH₂Cl₂, 30 min

5: 95 percent / aq. NaOH / 0.5 h / Ambient temperature

With manganese(IV) oxide; sodium hydroxide; hydrogen; palladium hydroxide - carbon; In dichloromethane; ethyl acetate;