C₄₃H₄₉N₅O₉S

Base Information

Chemical Name:C₄₃H₄₉N₅O₉S
CAS No.:1275618-99-9
Molecular Formula:C₄₃H₄₉N₅O₉S
Molecular Weight:811.956
Hs Code.:

C<sub>43</sub>H<sub>49</sub>N<sub>5</sub>O<sub>9</sub>S

Synonyms:C₄₃H₄₉N₅O₉S

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Chemical Property of C₄₃H₄₉N₅O₉S

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Technology Process of C₄₃H₄₉N₅O₉S

There total 13 articles about C₄₃H₄₉N₅O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1275620-49-9
C₄₅H₅₃N₅O₉S

: 1275618-99-9
C₄₃H₄₉N₅O₉S

Guidance literature:: Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 40 ℃; for 24h; Inert atmosphere;

Reference yield:

: 1275620-46-6
C₂₃H₂₀N₂O₄

: 1275618-99-9
C₄₃H₄₉N₅O₉S

Guidance literature:: Multi-step reaction with 4 steps

1.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C

2.1: lithium hydroxide / tetrahydrofuran / 20 °C

2.2: pH < 7

3.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C

4.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 24 h / 40 °C / Inert atmosphere

With 4-methyl-morpholine; benzotriazol-1-ol; HATU; lithium hydroxide; Hoveyda-Grubbs catalyst second generation; In tetrahydrofuran; dichloromethane;

Reference yield:

: 49615-96-5
1-(3-aminobenzofuran-2-yl)ethan-1-one

: 1275618-99-9
C₄₃H₄₉N₅O₉S

Guidance literature:: Multi-step reaction with 12 steps

1.1: ethanol; water / 5 - 10 °C

2.1: Warmed water bath

3.1: bromine / chloroform

4.1: potassium acetate / acetone

5.1: acetic acid; phosphoric acid / 5 h / Reflux

6.1: trichlorophosphate / 2 h / Reflux

7.1: sodium t-butanolate / dimethyl sulfoxide / 1 h / 0 - 20 °C

7.2: 4 h / 10 °C

7.3: pH 6 - 7

8.1: thionyl chloride / 1 h / Reflux

9.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C

10.1: lithium hydroxide / tetrahydrofuran / 20 °C

10.2: pH < 7

11.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C

12.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 24 h / 40 °C / Inert atmosphere

With 4-methyl-morpholine; thionyl chloride; phosphoric acid; bromine; potassium acetate; benzotriazol-1-ol; acetic acid; HATU; lithium hydroxide; sodium t-butanolate; trichlorophosphate; Hoveyda-Grubbs catalyst second generation; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; dimethyl sulfoxide; acetone;