6-pentylundec-5-ene

Base Information

• Chemical Name: 6-pentylundec-5-ene
• CAS No.: 51677-36-2
• Molecular Formula: C16H32
• Molecular Weight: 224.43
• Mol file: 51677-36-2.mol

Synonyms:

Chemical Property of 6-pentylundec-5-ene

Chemical Property:

• Vapor Pressure: 0.0043mmHg at 25°C
• Boiling Point: 287.4°Cat760mmHg
• Flash Point: 92.2°C
• Density: 0.784g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-pentylundec-5-ene

There total 10 articles about 6-pentylundec-5-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

dipentyl ketone (927-49-1) → 6-pentyl-5-undecene (51677-36-2)

Guidance literature:

With boron trifluoride diethyl etherate; ethylene glycol; In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4020(01)81545-3

Reference yield: 30.0%

3,3-dipentyl-2-oxooctanoic acid (26269-42-1) → 6-pentyl-5-undecene (51677-36-2) + 2,2-dipentyl-heptanoic acid (52061-77-5)

Guidance literature:

With quinoline; oxygen; cobalt(II) acetate; copper; at 150 ℃; for 2.5h;

DOI:10.1021/jo00159a038

Reference yield:

6-chloro-6-pentyl-undecane (51677-37-3) → 6-pentyl-5-undecene (51677-36-2) + Tri-n-pentylmethyl-Azide (51677-32-8)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 95 - 100 ℃; for 60h;

DOI:10.1021/ja00809a025

upstream raw materials:

6-pentyl-undecan-6-ol

6-chloro-6-pentyl-undecane

dipentyl ketone

3,3-dipentyl-2-oxooctanoic acid

Downstream raw materials:

pentanal

dipentyl ketone

Refernces

• 1、 Nagumo, Shinji,Matsukuma, Aki,Suemune, Hiroshi,Sakai, Kiyoshi. "Novel Ring Cleavage Based on Intermolecular Aldol Condensation". . p. 10501 - 10510. Retrieved 2007/10/02.