2,5,6-triamino-1-methyl-4-pyrimidone sulfate

Base Information

• Chemical Name: 2,5,6-triamino-1-methyl-4-pyrimidone sulfate
• CAS No.: 1130-04-7
• Molecular Formula: C₅H₉N₅O*H₂O₄S
• Molecular Weight: 253.239
• Mol file: 1130-04-7.mol

Synonyms:2,5,6-triamino-1-methyl-4-pyrimidone sulfate

Chemical Property of 2,5,6-triamino-1-methyl-4-pyrimidone sulfate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,5,6-triamino-1-methyl-4-pyrimidone sulfate

There total 2 articles about 2,5,6-triamino-1-methyl-4-pyrimidone sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2,6-diamino-1-methyl-5-nitroso-4-pyrimidone (58160-46-6) → 2,5,6-triamino-1-methyl-4-pyrimidone sulfate (1130-04-7)

Guidance literature:

With sodium dithionite;

Reference yield:

2,6-diamino-1-methyl-4-pyrimidone hemihydrochloride (84321-38-0) → 2,5,6-triamino-1-methyl-4-pyrimidone sulfate (1130-04-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / HNO₂

2: 71 percent / Na₂S₂O₄

With sodium dithionite; cis-nitrous acid;

Reference yield: 57.0%

2,5,6-triamino-1-methyl-4-pyrimidone sulfate (1130-04-7) + formamide (77287-34-4,77287-35-5,60100-09-6) → 3-methylguanine (2958-98-7)

Guidance literature:

at 150 ℃; for 4h;

upstream raw materials:

2,6-diamino-1-methyl-5-nitroso-4-pyrimidone

2,6-diamino-1-methyl-4-pyrimidone hemihydrochloride

Downstream raw materials:

3-methylguanine