(2S)-2-({[4-(2-butynyloxy)phenyl]-sulfonyl}amino)-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid

Base Information

Chemical Name:(2S)-2-({[4-(2-butynyloxy)phenyl]-sulfonyl}amino)-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid
CAS No.:287407-34-5
Molecular Formula:C₁₈H₂₅NO₆S₂
Molecular Weight:415.532
Hs Code.:

Synonyms:(2S)-2-({[4-(2-butynyloxy)phenyl]-sulfonyl}amino)-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid

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Chemical Property of (2S)-2-({[4-(2-butynyloxy)phenyl]-sulfonyl}amino)-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid

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Technology Process of (2S)-2-({[4-(2-butynyloxy)phenyl]-sulfonyl}amino)-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid

There total 2 articles about (2S)-2-({[4-(2-butynyloxy)phenyl]-sulfonyl}amino)-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 287407-33-4
(2S)-2-amino-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid

: 286459-94-7
4-but-2-ynyloxybenzenesulfonyl chloride

: 287407-34-5
(2S)-2-({[4-(2-butynyloxy)phenyl]-sulfonyl}amino)-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid

Guidance literature:: (2S)-2-amino-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid; 4-but-2-ynyloxybenzenesulfonyl chloride; With triethylamine; In 1,4-dioxane; water; at 20 ℃; for 15h;

With hydrogenchloride; In 1,4-dioxane; water; pH=2;

Reference yield:

: 2-butynyloxybenzenesulfonyl chloride

: 287407-33-4
(2S)-2-amino-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid

: 287407-34-5
(2S)-2-({[4-(2-butynyloxy)phenyl]-sulfonyl}amino)-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid

Guidance literature:: With triethylamine; In 1,4-dioxane; water;

Reference yield: 88.0%

: 287407-34-5
(2S)-2-({[4-(2-butynyloxy)phenyl]-sulfonyl}amino)-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid

: (2S)-2-({[4-(2-Butynyloxy)phenyl]sulfonyl}amino)-N-hydroxy-3-[(3-hydroxy-propyl)sulfanyl]-3-methylbutanamide

Guidance literature:: (2S)-2-({[4-(2-butynyloxy)phenyl]-sulfonyl}amino)-3-[(3-hydroxypropyl)sulfanyl]-3-methylbutanoic acid; With 4-methyl-morpholine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 1h;

With hydroxylamine; In water; at 20 ℃; for 15h;