N-(2,5-Dimethoxyphenyl)-2-nitro-beta-oxobenzenepropanamide

Base Information

Chemical Name:N-(2,5-Dimethoxyphenyl)-2-nitro-beta-oxobenzenepropanamide
CAS No.:122022-06-4
Molecular Formula:C₁₇H₁₆N₂O₆
Molecular Weight:344.324
Hs Code.:
DSSTox Substance ID:DTXSID901205452
Nikkaji Number:J765.130I

Synonyms:DTXSID901205452;122022-06-4

Suppliers and Price of N-(2,5-Dimethoxyphenyl)-2-nitro-beta-oxobenzenepropanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,5-Dimethoxyphenyl)-2-nitro-beta-oxobenzenepropanamide

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:344.10083623
Heavy Atom Count:25
Complexity:492

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)OC)NC(=O)CC(=O)C2=CC=CC=C2[N+](=O)[O-]

Technology Process of N-(2,5-Dimethoxyphenyl)-2-nitro-beta-oxobenzenepropanamide

There total 1 articles about N-(2,5-Dimethoxyphenyl)-2-nitro-beta-oxobenzenepropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52119-39-8
ethyl (2-nitrobenzoyl)acetate

: 102-56-7,102526-87-4
2,5-dimethoxyaniline

: 122022-06-4
2,5-dimethoxy(2-nitrobenzoyl)acetanilide

Guidance literature:: With pyridine; In toluene; at 140 ℃; for 6h;
DOI:10.3987/COM-88-4653

Reference yield: 53.0%

: 122022-06-4
2,5-dimethoxy(2-nitrobenzoyl)acetanilide

: 121998-60-5
5,8-Dimethoxy-4-(2-nitrophenyl)-2(1H)-quinolinone

Guidance literature:: With sulfuric acid; at 75 ℃; for 0.5h;
DOI:10.3987/COM-88-4653

Reference yield:

: 122022-06-4
2,5-dimethoxy(2-nitrobenzoyl)acetanilide

: 121998-62-7
2-Chloro-4-(2-nitro-phenyl)-quinoline-5,8-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / 80percent H₂SO₄ / 0.5 h / 75 °C

2: 94 percent / POCl₃ / dimethylformamide / 3 h / 90 °C

3: 77 percent / CAN / H₂O; acetonitrile / 0.25 h / 0 °C

With ammonium cerium(IV) nitrate; sulfuric acid; trichlorophosphate; In water; N,N-dimethyl-formamide; acetonitrile;