3-(2-iodophenyl)propanoyl chloride

Base Information

Chemical Name:3-(2-iodophenyl)propanoyl chloride
CAS No.:897660-99-0
Molecular Formula:C₉H₈ClIO
Molecular Weight:294.519
Hs Code.:

Synonyms:3-(2-iodophenyl)propanoyl chloride

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Chemical Property of 3-(2-iodophenyl)propanoyl chloride

Chemical Property:

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Technology Process of 3-(2-iodophenyl)propanoyl chloride

There total 4 articles about 3-(2-iodophenyl)propanoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26260-02-6
2-iodobenzaldehyde

: 897660-99-0
3-(2-iodophenyl)propanoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid; triethylammonium formate

2: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 3 h / Inert atmosphere; Reflux

With formic acid; thionyl chloride; triethylammonium formate; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1002/adsc.201000044

Reference yield:

: 5159-41-1
2-iodobenzyl alcohol

: 897660-99-0
3-(2-iodophenyl)propanoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: silica gel; dipyridinium dichromate / dichloromethane / 6 h / 20 °C / Inert atmosphere

2.1: triethylamine; formic acid / N,N-dimethyl-formamide / 12 h / 65 °C / Inert atmosphere

2.2: 6 h / 90 °C / Inert atmosphere

3.1: oxalyl dichloride; N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With dipyridinium dichromate; formic acid; oxalyl dichloride; silica gel; triethylamine; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.7b03577

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 897660-99-0
3-(2-iodophenyl)propanoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: Trimethyl borate; dimethylsulfide borane complex / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

2.1: silica gel; dipyridinium dichromate / dichloromethane / 6 h / 20 °C / Inert atmosphere

3.1: triethylamine; formic acid / N,N-dimethyl-formamide / 12 h / 65 °C / Inert atmosphere

3.2: 6 h / 90 °C / Inert atmosphere

4.1: oxalyl dichloride; N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

With dipyridinium dichromate; formic acid; oxalyl dichloride; Trimethyl borate; dimethylsulfide borane complex; silica gel; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.7b03577