Technology Process of (1S,3S)-3-acetyl-2,2-dimethylcyclobutaneacetaldehyde1,6-cyclodecanedione
There total 9 articles about (1S,3S)-3-acetyl-2,2-dimethylcyclobutaneacetaldehyde1,6-cyclodecanedione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(+)-α-pinene;
With
ozone;
In
dichloromethane; isopropyl alcohol;
at -78 ℃;
With
ring-opening metathesis polymer-supported triphenylphosphine;
In
dichloromethane; isopropyl alcohol;
at 20 ℃;
for 2h;
Further stages.;
DOI:10.1021/ol026008q
- Guidance literature:
-
With
C21H12Cl6NO4V; oxygen;
In
toluene;
at 1000 ℃;
for 1.5h;
under 760.051 Torr;
Reagent/catalyst;
chemoselective reaction;
DOI:10.1002/adsc.201800050
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
water; ethyl acetate; acetone;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/jacs.1c07509