Technology Process of C10H15OPS
There total 10 articles about C10H15OPS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: iodoxybenzene / chloroform / 20 °C
2: borane-THF / tetrahydrofuran / 20 °C
3: oct-1-ene; sulfur / tetrahydrofuran / Reflux
4: iodoxybenzene / chloroform / 20 °C
5: triethylamine / dichloromethane / 96 h / 20 °C
6: sodium iodide / acetone / 336 h / Reflux
7: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 192 h / Reflux
8: borane-THF / tetrahydrofuran / 20 °C
9: oct-1-ene; sulfur / tetrahydrofuran / Reflux
With
borane-THF; 2,2'-azobis(isobutyronitrile); oct-1-ene; iodoxybenzene; tri-n-butyl-tin hydride; sulfur; triethylamine; sodium iodide;
In
tetrahydrofuran; dichloromethane; chloroform; acetone; benzene;
DOI:10.1016/j.tetasy.2011.08.024
- Guidance literature:
-
Multi-step reaction with 7 steps
1: oct-1-ene; sulfur / tetrahydrofuran / Reflux
2: iodoxybenzene / chloroform / 20 °C
3: triethylamine / dichloromethane / 96 h / 20 °C
4: sodium iodide / acetone / 336 h / Reflux
5: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 192 h / Reflux
6: borane-THF / tetrahydrofuran / 20 °C
7: oct-1-ene; sulfur / tetrahydrofuran / Reflux
With
borane-THF; 2,2'-azobis(isobutyronitrile); oct-1-ene; iodoxybenzene; tri-n-butyl-tin hydride; sulfur; triethylamine; sodium iodide;
In
tetrahydrofuran; dichloromethane; chloroform; acetone; benzene;
DOI:10.1016/j.tetasy.2011.08.024