N-(3-azidopropyl)-4'-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-[1,1'-biphenyl]-4-carboxamide

Base Information

Chemical Name:N-(3-azidopropyl)-4'-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-[1,1'-biphenyl]-4-carboxamide
CAS No.:1310048-48-6
Molecular Formula:C₂₄H₂₅N₅O₄
Molecular Weight:447.494
Hs Code.:

Synonyms:N-(3-azidopropyl)-4'-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-[1,1'-biphenyl]-4-carboxamide

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Chemical Property of N-(3-azidopropyl)-4'-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-[1,1'-biphenyl]-4-carboxamide

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Technology Process of N-(3-azidopropyl)-4'-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-[1,1'-biphenyl]-4-carboxamide

There total 2 articles about N-(3-azidopropyl)-4'-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-[1,1'-biphenyl]-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1310048-47-5
4'-amino-N-(3-azidopropyl)-[1,1'-biphenyl]-4-carboxamide

: 95298-68-3
3-methoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid

: 1310048-48-6
N-(3-azidopropyl)-4'-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-[1,1'-biphenyl]-4-carboxamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 120 ℃; for 0.5h; Inert atmosphere; Microwave irradiation;
DOI:10.1002/anie.201007871

Reference yield:

: 5730-78-9
4-(4-aminophenyl)benzoic acid

: 1310048-48-6
N-(3-azidopropyl)-4'-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-[1,1'-biphenyl]-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0.5 h / 120 °C / Inert atmosphere; Microwave irradiation

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0.5 h / 120 °C / Inert atmosphere; Microwave irradiation

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1002/anie.201007871

Reference yield: 85.0%

: 1310048-48-6
N-(3-azidopropyl)-4'-(3-methoxy-5-oxocyclohex-3-enecarboxamido)-[1,1'-biphenyl]-4-carboxamide

: 1310048-37-3
C₂₃H₂₃N₅O₄

Guidance literature:: With ammonium cerium (IV) nitrate; water; In acetonitrile; at 95 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.201007871