N-[(1S,3S)-1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carbonyl]-N'-tyrosylhydrazine

Base Information

Chemical Name:N-[(1S,3S)-1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carbonyl]-N'-tyrosylhydrazine
CAS No.:1313586-22-9
Molecular Formula:C₂₂H₂₅N₅O₃
Molecular Weight:407.472
Hs Code.:

Synonyms:N-[(1S,3S)-1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carbonyl]-N'-tyrosylhydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(1S,3S)-1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carbonyl]-N'-tyrosylhydrazine

Chemical Property:

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Technology Process of N-[(1S,3S)-1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carbonyl]-N'-tyrosylhydrazine

There total 4 articles about N-[(1S,3S)-1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carbonyl]-N'-tyrosylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1313586-04-7
N-[(1S,3S)-1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carbonyl]-N'-(Boc-tyrosyl)hydrazine

: 1313586-22-9
N-[(1S,3S)-1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carbonyl]-N'-tyrosylhydrazine

Guidance literature:: With hydrogenchloride; In water; ethyl acetate; Cooling;
DOI:10.1016/j.ejmech.2011.04.037

Reference yield:

: 191279-37-5,827304-63-2
(3S)-1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid

: 1313586-22-9
N-[(1S,3S)-1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carbonyl]-N'-tyrosylhydrazine

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 12 h / 20 °C

2: hydrazine hydrate / chloroform / 20 - 60 °C

3: 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C / Cooling

4: hydrogenchloride / water; ethyl acetate / Cooling

With 4-methyl-morpholine; hydrogenchloride; thionyl chloride; benzotriazol-1-ol; hydrazine hydrate; dicyclohexyl-carbodiimide; In tetrahydrofuran; chloroform; water; ethyl acetate;
DOI:10.1016/j.ejmech.2011.04.037

Reference yield:

: 191279-38-6
(3S)-1-methyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-3-carboxylic acid methyl ester

: 1313586-22-9
N-[(1S,3S)-1-methyl-1,2,3,4-tetrahydro-β-carboline-3-carbonyl]-N'-tyrosylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / chloroform / 20 - 60 °C

2: 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C / Cooling

3: hydrogenchloride / water; ethyl acetate / Cooling

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; hydrazine hydrate; dicyclohexyl-carbodiimide; In tetrahydrofuran; chloroform; water; ethyl acetate;
DOI:10.1016/j.ejmech.2011.04.037