(4S,2'S,3'R)-3'-<3'-((benzyloxy)methoxy)-2'-methylpentanoyl>-4-isopropyl-1,3-oxazolidin-2-one

Base Information

Chemical Name:(4S,2'S,3'R)-3'-<3'-((benzyloxy)methoxy)-2'-methylpentanoyl>-4-isopropyl-1,3-oxazolidin-2-one
CAS No.:159102-42-8
Molecular Formula:C₂₀H₂₉NO₅
Molecular Weight:363.454
Hs Code.:

Synonyms:(4S,2'S,3'R)-3'-<3'-((benzyloxy)methoxy)-2'-methylpentanoyl>-4-isopropyl-1,3-oxazolidin-2-one

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Chemical Property of (4S,2'S,3'R)-3'-<3'-((benzyloxy)methoxy)-2'-methylpentanoyl>-4-isopropyl-1,3-oxazolidin-2-one

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Technology Process of (4S,2'S,3'R)-3'-<3'-((benzyloxy)methoxy)-2'-methylpentanoyl>-4-isopropyl-1,3-oxazolidin-2-one

There total 2 articles about (4S,2'S,3'R)-3'-<3'-((benzyloxy)methoxy)-2'-methylpentanoyl>-4-isopropyl-1,3-oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3587-60-8
Benzyloxymethyl chloride

: 88636-00-4
(4S)-3-<(2'S,3'R)-3'-hydroxy-2'-methylpentanoyl>-4-isopropyl-1,3-oxazolidin-2-one

: 159102-42-8
(4S,2'S,3'R)-3'-<3'-((benzyloxy)methoxy)-2'-methylpentanoyl>-4-isopropyl-1,3-oxazolidin-2-one

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 45h; Ambient temperature;
DOI:10.1021/ja00090a016

Reference yield:

: 77877-19-1,165657-81-8
N-isopropyl oxazolidinone

: 159102-42-8
(4S,2'S,3'R)-3'-<3'-((benzyloxy)methoxy)-2'-methylpentanoyl>-4-isopropyl-1,3-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) (n-Bu)2BOTf, Et₃N, 3.) 30percent aq. H₂O₂

2: 91 percent / i-Pr₂NEt / CH₂Cl₂ / 45 h / Ambient temperature

With di-n-butylboryl trifluoromethanesulfonate; dihydrogen peroxide; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/ja00090a016

Reference yield: 92.0%

: 159102-42-8
(4S,2'S,3'R)-3'-<3'-((benzyloxy)methoxy)-2'-methylpentanoyl>-4-isopropyl-1,3-oxazolidin-2-one

: 159102-43-9
(2R,3R)-3-<(benzyloxy)methoxy>-2-methylpentanol

Guidance literature:: With lithium borohydride; In tetrahydrofuran; diethyl ether; water; for 2h; Ambient temperature;
DOI:10.1021/ja00090a016