bis(diphenylphosphino)methane borane

Base Information

Chemical Name:bis(diphenylphosphino)methane borane
CAS No.:104413-76-5
Molecular Formula:C₂₅H₂₅BP₂
Molecular Weight:398.232
Hs Code.:

Synonyms:bis(diphenylphosphino)methane borane

Suppliers and Price of bis(diphenylphosphino)methane borane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bis(diphenylphosphino)methane borane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bis(diphenylphosphino)methane borane

There total 1 articles about bis(diphenylphosphino)methane borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.4%

: 16940-66-2
sodium tetrahydroborate

: 2071-20-7
bis-diphenylphosphinomethane

: 104413-76-5
bis(diphenylphosphino)methane borane

Guidance literature:: With I₂; In 1,2-dimethoxyethane; byproducts: NaI; dropwise addn. of I2 (2.5mmol) and bis(diphenylphosphino)methane (5mmol) in glyme to NaBH4 (10mmol) in glyme with stirring; pptn., stirring for1h; removal of solvent in vac., filtration of benzene suspension; evapn.; addn. of dry hexane, pptn.; drying overnight under vac.; elem. anal.;
DOI:10.1016/S0020-1693(00)87690-2

Reference yield: 94.0%

: tris(acetonitrile)pentamethylcyclopentadienylruthenium(II) hexafluorophosphate

: 104413-76-5
bis(diphenylphosphino)methane borane

: [(η5-C5Me5)Ru(η2-Ph2PCH2Ph2P*BH3)][PF6]

Guidance literature:: In acetonitrile; (Ar); stirred for 30 min at room temp.; evapd. (vac.), crystd. from CD2Cl2/hexane; elem. anal.;
DOI:10.1039/b413650k