(8E)-1-tert-butyldimethylsilyoxy-6,6-diethoxycarbonyl-7-methylene-9-phenyl-8-nonene

Base Information

Chemical Name:(8E)-1-tert-butyldimethylsilyoxy-6,6-diethoxycarbonyl-7-methylene-9-phenyl-8-nonene
CAS No.:1223582-54-4
Molecular Formula:C₂₈H₄₄O₅Si
Molecular Weight:488.74
Hs Code.:

Synonyms:(8E)-1-tert-butyldimethylsilyoxy-6,6-diethoxycarbonyl-7-methylene-9-phenyl-8-nonene

Suppliers and Price of (8E)-1-tert-butyldimethylsilyoxy-6,6-diethoxycarbonyl-7-methylene-9-phenyl-8-nonene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (8E)-1-tert-butyldimethylsilyoxy-6,6-diethoxycarbonyl-7-methylene-9-phenyl-8-nonene

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Technology Process of (8E)-1-tert-butyldimethylsilyoxy-6,6-diethoxycarbonyl-7-methylene-9-phenyl-8-nonene

There total 1 articles about (8E)-1-tert-butyldimethylsilyoxy-6,6-diethoxycarbonyl-7-methylene-9-phenyl-8-nonene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 960283-15-2
(4E)-ethyl 2-ethoxycarbonyl-3-methylene-5-phenyl-4-pentenoate

: 85514-45-0
tert-butyl((5-iodopentyl)oxy)dimethylsilane

: 1223582-54-4
(8E)-1-tert-butyldimethylsilyoxy-6,6-diethoxycarbonyl-7-methylene-9-phenyl-8-nonene

Guidance literature:: (4E)-ethyl 2-ethoxycarbonyl-3-methylene-5-phenyl-4-pentenoate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

tert-butyl((5-iodopentyl)oxy)dimethylsilane; In N,N-dimethyl-formamide; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.013

Reference yield: 87.0%

: 1223582-54-4
(8E)-1-tert-butyldimethylsilyoxy-6,6-diethoxycarbonyl-7-methylene-9-phenyl-8-nonene

: 1223582-55-5
(8E)-6,6-diethoxycarbonyl-7-methylene-9-phenylnon-8-en-1-ol

Guidance literature:: With water; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.013