ethyl 7-(3,5-dichloro-4-((2,4-dichlorophenyl)(hydroxy)methyl)phenoxy)heptanoate

Base Information

Chemical Name:ethyl 7-(3,5-dichloro-4-((2,4-dichlorophenyl)(hydroxy)methyl)phenoxy)heptanoate
CAS No.:934562-63-7
Molecular Formula:C₂₂H₂₄Cl₄O₄
Molecular Weight:494.242
Hs Code.:

Synonyms:ethyl 7-(3,5-dichloro-4-((2,4-dichlorophenyl)(hydroxy)methyl)phenoxy)heptanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 7-(3,5-dichloro-4-((2,4-dichlorophenyl)(hydroxy)methyl)phenoxy)heptanoate

Chemical Property:

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Technology Process of ethyl 7-(3,5-dichloro-4-((2,4-dichlorophenyl)(hydroxy)methyl)phenoxy)heptanoate

There total 5 articles about ethyl 7-(3,5-dichloro-4-((2,4-dichlorophenyl)(hydroxy)methyl)phenoxy)heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 934562-72-8
ethyl 7-(3,5-dichloro-4-(2,4-dichlorobenzoyl)phenoxy)heptanoate

: 934562-63-7
ethyl 7-(3,5-dichloro-4-((2,4-dichlorophenyl)(hydroxy)methyl)phenoxy)heptanoate

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃;
DOI:10.1021/ol070150f

Reference yield:

: 934562-64-8
(2,6-dichloro-4-methoxyphenyl)(2,4-dichlorophenyl)methanone

: 934562-63-7
ethyl 7-(3,5-dichloro-4-((2,4-dichlorophenyl)(hydroxy)methyl)phenoxy)heptanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / aq. HBr; AcOH / 6 h / 110 °C

2: 95 percent / potassium carbonate / dimethylformamide / 12 h / 20 °C

3: 98 percent / NaBH₄ / methanol / 0 °C

With sodium tetrahydroborate; hydrogen bromide; potassium carbonate; acetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ol070150f

Reference yield:

: 74390-79-7
(2,6-dichloro-4-hydroxyphenyl)(2,4-dichlorophenyl)methanone

: 934562-63-7
ethyl 7-(3,5-dichloro-4-((2,4-dichlorophenyl)(hydroxy)methyl)phenoxy)heptanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / potassium carbonate / dimethylformamide / 12 h / 20 °C

2: 98 percent / NaBH₄ / methanol / 0 °C

With sodium tetrahydroborate; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ol070150f