2-(t-butylamino)-4'-hydroxy-3'-(methylsulfinyl)acetophenone methanesulfonate

Base Information

Chemical Name:2-(t-butylamino)-4'-hydroxy-3'-(methylsulfinyl)acetophenone methanesulfonate
CAS No.:69181-41-5
Molecular Formula:CH₄O₃S*C₁₃H₁₉NO₃S
Molecular Weight:365.472
Hs Code.:

Synonyms:2-(t-butylamino)-4'-hydroxy-3'-(methylsulfinyl)acetophenone methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(t-butylamino)-4'-hydroxy-3'-(methylsulfinyl)acetophenone methanesulfonate

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Technology Process of 2-(t-butylamino)-4'-hydroxy-3'-(methylsulfinyl)acetophenone methanesulfonate

There total 5 articles about 2-(t-butylamino)-4'-hydroxy-3'-(methylsulfinyl)acetophenone methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69181-39-1
2-(tert-butylamino)-4'-hydroxy-3'-(methylthio)acetophenone 4'-acetate

: 69181-41-5
2-(t-butylamino)-4'-hydroxy-3'-(methylsulfinyl)acetophenone methanesulfonate

Guidance literature:: With dihydrogen peroxide; In methanol; dichloromethane;

Reference yield:

: 1073-29-6
2-(methylsulfenyl)phenol

: 69181-41-5
2-(t-butylamino)-4'-hydroxy-3'-(methylsulfinyl)acetophenone methanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: aluminium trichloride / nitrobenzene

2: triethylamine / dichloromethane

3: bromine; calcium carbonate / chloroform

4: hydrogenchloride; tert-butylamine / N,N-dimethyl-formamide

5: dihydrogen peroxide / methanol; dichloromethane

With hydrogenchloride; dihydrogen peroxide; bromine; tert-butylamine; triethylamine; calcium carbonate; aluminium trichloride; In methanol; dichloromethane; chloroform; nitrobenzene; N,N-dimethyl-formamide;

Reference yield:

: 66264-56-0
1-[4-hydroxy-3-(methylmercapto)phenyl]-ethanone

: 69181-41-5
2-(t-butylamino)-4'-hydroxy-3'-(methylsulfinyl)acetophenone methanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane

2: bromine; calcium carbonate / chloroform

3: hydrogenchloride; tert-butylamine / N,N-dimethyl-formamide

4: dihydrogen peroxide / methanol; dichloromethane

With hydrogenchloride; dihydrogen peroxide; bromine; tert-butylamine; triethylamine; calcium carbonate; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide;