7-<<<2-(hydroxymethyl)phenyl>thio>methyl>-6-hydroxy-1,2,3,4-tetrahydrobenzopyran

Base Information

Chemical Name:7-<<<2-(hydroxymethyl)phenyl>thio>methyl>-6-hydroxy-1,2,3,4-tetrahydrobenzopyran
CAS No.:103447-31-0
Molecular Formula:C₁₇H₁₈O₃S
Molecular Weight:302.394
Hs Code.:

Synonyms:7-<<<2-(hydroxymethyl)phenyl>thio>methyl>-6-hydroxy-1,2,3,4-tetrahydrobenzopyran

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Chemical Property of 7-<<<2-(hydroxymethyl)phenyl>thio>methyl>-6-hydroxy-1,2,3,4-tetrahydrobenzopyran

Chemical Property:

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Technology Process of 7-<<<2-(hydroxymethyl)phenyl>thio>methyl>-6-hydroxy-1,2,3,4-tetrahydrobenzopyran

There total 8 articles about 7-<<<2-(hydroxymethyl)phenyl>thio>methyl>-6-hydroxy-1,2,3,4-tetrahydrobenzopyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4521-31-7
o-hydroxymethyl thiophenol

: 103447-30-9
6-hydroxy-7-(hydroxymethyl)-1,2,3,4-tetrahydrobenzopyran diacetate

: 103447-31-0
7-<<<2-(hydroxymethyl)phenyl>thio>methyl>-6-hydroxy-1,2,3,4-tetrahydrobenzopyran

Guidance literature:: With sodium hydroxide; In N-methyl-acetamide; hexane; mineral oil;

Reference yield:

: Acetic acid 7-(2-hydroxymethyl-phenylsulfanylmethyl)-chroman-6-yl ester

: 103447-31-0
7-<<<2-(hydroxymethyl)phenyl>thio>methyl>-6-hydroxy-1,2,3,4-tetrahydrobenzopyran

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; Yield given; Ambient temperature;

Reference yield:

: 4521-31-7
o-hydroxymethyl thiophenol

: 103447-31-0
7-<<<2-(hydroxymethyl)phenyl>thio>methyl>-6-hydroxy-1,2,3,4-tetrahydrobenzopyran

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 30 min, 2.) a) RT, 3 h, b) 50 deg, 30 min

2: 2.5 NaOH / dimethylformamide / Ambient temperature

With sodium hydroxide; sodium hydride; In N,N-dimethyl-formamide;