N⁶-[(benzyloxy)carbonyl]-N²-{N ²,N⁶-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine

Base Information

• Chemical Name: N⁶-[(benzyloxy)carbonyl]-N²-{N ²,N⁶-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine
• CAS No.: 614-02-8
• Molecular Formula: C₃₆H₄₄N₄O₉
• Molecular Weight: 676.767

Synonyms:N⁶-[(benzyloxy)carbonyl]-N²-{N ²,N⁶-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine

Chemical Property of N⁶-[(benzyloxy)carbonyl]-N²-{N ²,N⁶-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine

Chemical Property:

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Technology Process of N⁶-[(benzyloxy)carbonyl]-N²-{N ²,N⁶-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine

There total 10 articles about N⁶-[(benzyloxy)carbonyl]-N²-{N ²,N⁶-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nα,Nε-Bis(benzyloxycarbonyl)-L-lysyl-Nε-(benzyloxycarbonyl)-L-lysine Methyl Ester (13523-84-7,97485-07-9) → N6-[(benzyloxy)carbonyl]-N2-{N 2,N6-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine (614-02-8)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/ja01152a519

Reference yield:

dilysine (13184-13-9) + benzyl 4-nitrophenyl carbonate (13795-24-9) → N6-[(benzyloxy)carbonyl]-N2-{N 2,N6-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine (614-02-8)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; at 20 ℃;

Reference yield:

N2-L-lysyl-L-lysine dihydrochloride (52123-30-5,57282-52-7,73343-51-8,134276-45-2) + dibenzyl dicarbonate (31139-36-3) → N6-[(benzyloxy)carbonyl]-N2-{N 2,N6-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine (614-02-8)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; at 20 ℃;

upstream raw materials:

N^α,N^ε-Bis(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine Methyl Ester

N,N'-di-[(phenylmethoxy)carbonyl]-L-lysine

(S)-methyl 2-amino-6-(benzyloxycarbonylamino)hexanoate

methyl (2S)-2-amino-6-{[(benzyloxy)carbonyl]amino}hexanoate hydrochloride

Downstream raw materials:

N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine

C₆₅H₁₀₁N₇O₁₀

N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester

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