C₂₈H₂₆FN₆O₆PS

Base Information

Chemical Name:C₂₈H₂₆FN₆O₆PS
CAS No.:1407520-39-1
Molecular Formula:C₂₈H₂₆FN₆O₆PS
Molecular Weight:624.589
Hs Code.:

C<sub>28</sub>H<sub>26</sub>FN<sub>6</sub>O<sub>6</sub>PS

Synonyms:C₂₈H₂₆FN₆O₆PS

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Chemical Property of C₂₈H₂₆FN₆O₆PS

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Technology Process of C₂₈H₂₆FN₆O₆PS

There total 5 articles about C₂₈H₂₆FN₆O₆PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1407520-38-0
C₂₁H₁₉ClFN₄O₃PS

: 99-59-2
3-amino-4-methoxynitrobenzene

: 1407520-39-1
C₂₈H₂₆FN₆O₆PS

Guidance literature:: With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; tert-butyl alcohol; at 110 ℃; Inert atmosphere;

Reference yield:

: 615-43-0
2-iodophenylamine

: 1407520-39-1
C₂₈H₂₆FN₆O₆PS

Guidance literature:: Multi-step reaction with 3 steps

1: potassium phosphate / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / N,N-dimethyl-formamide / 3 h / 150 °C

2: hydrogenchloride / isopropyl alcohol; 1,4-dioxane / 2 h / 150 °C / Microwave irradiation

3: sodium t-butanolate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene; tert-butyl alcohol / 110 °C / Inert atmosphere

With hydrogenchloride; potassium phosphate; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; N,N-dimethyl-formamide; isopropyl alcohol; toluene; tert-butyl alcohol;

Reference yield:

: 90213-66-4
2,4-dichloro-7H-pyrrolo[2,3-d]pyrimidine

: 1407520-39-1
C₂₈H₂₆FN₆O₆PS

Guidance literature:: Multi-step reaction with 4 steps

1.1: Selectfluor; acetic acid / acetonitrile / 60 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C

2.2: 0.5 h / 0 - 20 °C

3.1: hydrogenchloride / isopropyl alcohol; 1,4-dioxane / 2 h / 150 °C / Microwave irradiation

4.1: sodium t-butanolate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene; tert-butyl alcohol / 110 °C / Inert atmosphere

With hydrogenchloride; sodium hydride; acetic acid; Selectfluor; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; isopropyl alcohol; toluene; acetonitrile; mineral oil; tert-butyl alcohol;