2,4,6-triiodo-5-(2-[1,4,7,10-tetraazacyclododecanyl]-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-[1,4,7,10-tetraazacyclododecanyl])amide

Base Information

Chemical Name:2,4,6-triiodo-5-(2-[1,4,7,10-tetraazacyclododecanyl]-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-[1,4,7,10-tetraazacyclododecanyl])amide
CAS No.:869339-41-3
Molecular Formula:C₄₅H₈₂I₃N₁₇O₅
Molecular Weight:1321.97
Hs Code.:

2,4,6-triiodo-5-(2-[1,4,7,10-tetraazacyclododecanyl]-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-[1,4,7,10-tetraazacyclododecanyl])amide

Synonyms:2,4,6-triiodo-5-(2-[1,4,7,10-tetraazacyclododecanyl]-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-[1,4,7,10-tetraazacyclododecanyl])amide

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Chemical Property of 2,4,6-triiodo-5-(2-[1,4,7,10-tetraazacyclododecanyl]-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-[1,4,7,10-tetraazacyclododecanyl])amide

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Technology Process of 2,4,6-triiodo-5-(2-[1,4,7,10-tetraazacyclododecanyl]-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-[1,4,7,10-tetraazacyclododecanyl])amide

There total 1 articles about 2,4,6-triiodo-5-(2-[1,4,7,10-tetraazacyclododecanyl]-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-[1,4,7,10-tetraazacyclododecanyl])amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 869339-40-2
2,4,6-triiodo-5-(2-{10-[1,4,7-tris-(benzyloxycarbonyl)-1,4,7,10-tetraazacyclododecanyl]}-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-{10-[1,4,7-tris-(benzyloxycarbonyl)-1,4,7,10-tetraazacyclododecanyl]})amide

: 869339-41-3
2,4,6-triiodo-5-(2-[1,4,7,10-tetraazacyclododecanyl]-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-[1,4,7,10-tetraazacyclododecanyl])amide

Guidance literature:: 2,4,6-triiodo-5-(2-{10-[1,4,7-tris-(benzyloxycarbonyl)-1,4,7,10-tetraazacyclododecanyl]}-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-{10-[1,4,7-tris-(benzyloxycarbonyl)-1,4,7,10-tetraazacyclododecanyl]})amide; With hydrogen bromide; acetic acid; at 0 - 20 ℃; for 3h;

With sodium hydroxide; In dichloromethane; water; pH=10;

Reference yield: 67.0%

: 869339-41-3
2,4,6-triiodo-5-(2-[1,4,7,10-tetraazacyclododecanyl]-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-[1,4,7,10-tetraazacyclododecanyl])amide

: 79-11-8
chloroacetic acid

: 869339-42-4
2,4,6-triiodo-5-(2-{10-[1,4,7-tris-(carboxymethyl)-1,4,7,10-tetraazacyclododecanyl]}-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-{10-[1,4,7-tris-(carboxymethyl)-1,4,7,10-tetraazacyclododecanyl]})amide

Guidance literature:: 2,4,6-triiodo-5-(2-[1,4,7,10-tetraazacyclododecanyl]-propionyl)aminoisophthalic acid N,N-bis-(3-aza-5-methyl-4-oxopentane-1,5-diyl-[1,4,7,10-tetraazacyclododecanyl])amide; chloroacetic acid; With sodium hydroxide; In water; at 60 - 70 ℃; for 10h; pH=9.5;

With hydrogenchloride; In water; at 20 ℃; pH=1;