(2-hydroxy)phenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

Base Information

• Chemical Name: (2-hydroxy)phenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside
• CAS No.: 112965-26-1
• Molecular Formula: C₂₀H₂₄O₁₀S
• Molecular Weight: 456.471
• Mol file: 112965-26-1.mol

Synonyms:(2-hydroxy)phenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

Chemical Property of (2-hydroxy)phenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of (2-hydroxy)phenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

There total 2 articles about (2-hydroxy)phenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

ortho-mercaptophenol (1121-24-0) + β-D-glucose pentaacetate (604-69-3) → (2-hydroxy)phenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside (112965-26-1)

Guidance literature:

With boron trifluoride diethyl etherate; In acetone; at 0 - 20 ℃;

DOI:10.1039/b502990b

Reference yield:

→ (2-hydroxy)phenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside (112965-26-1)

Guidance literature:

α-Acetobromglucose, 2-Thiol-1-hydroxy-benzol ;

Reference yield:

(2-hydroxy)phenyl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside (112965-26-1) → C20H23O13S2(1-)*K(1+)

Guidance literature:

With sulfur trioxide pyridine complex; In dichloromethane; for 1h; Heating;

DOI:10.1039/b502990b

upstream raw materials:

ortho-mercaptophenol

β-D-glucose pentaacetate