C₂₈H₃₈N₈O₉S₂

Base Information

Chemical Name:C₂₈H₃₈N₈O₉S₂
CAS No.:1568826-52-7
Molecular Formula:C₂₈H₃₈N₈O₉S₂
Molecular Weight:694.79
Hs Code.:

C<sub>28</sub>H<sub>38</sub>N<sub>8</sub>O<sub>9</sub>S<sub>2</sub>

Synonyms:C₂₈H₃₈N₈O₉S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₃₈N₈O₉S₂

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Technology Process of C₂₈H₃₈N₈O₉S₂

There total 7 articles about C₂₈H₃₈N₈O₉S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1568826-40-3
C₂₉H₄₀N₈O₉S₂

: 1568826-52-7
C₂₈H₃₈N₈O₉S₂

Guidance literature:: With lithium hydroxide monohydrate; In tetrahydrofuran; water; at 20 - 50 ℃; for 24h;
DOI:10.1039/c3cc48850k

Reference yield:

: 1568825-98-8
methyl 2-(2-(2-bromo-2-methylpropanamido)phenylsulfonamido)-2-methylpropanoate

: 1568826-52-7
C₂₈H₃₈N₈O₉S₂

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide / N,N-dimethyl-formamide / 12 h / 70 °C

2: lithium hydroxide monohydrate / tetrahydrofuran; water / 24 h / 20 - 50 °C

3: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / acetonitrile / 12.17 h / 0 - 20 °C

4: lithium hydroxide monohydrate / tetrahydrofuran; water / 24 h / 20 - 50 °C

With sodium azide; lithium hydroxide monohydrate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c3cc48850k

Reference yield:

: 1401065-85-7
methyl-2-methyl-2-(2-nitrophenylsulfonamido) propanoate

: 1568826-52-7
C₂₈H₃₈N₈O₉S₂

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogen; palladium on activated charcoal / 12 h / 3102.97 Torr

2: triethylamine / dichloromethane / 12 h / 0 - 20 °C

3: sodium azide / N,N-dimethyl-formamide / 12 h / 70 °C

4: lithium hydroxide monohydrate / tetrahydrofuran; water / 24 h / 20 - 50 °C

5: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / acetonitrile / 12.17 h / 0 - 20 °C

6: lithium hydroxide monohydrate / tetrahydrofuran; water / 24 h / 20 - 50 °C

With sodium azide; lithium hydroxide monohydrate; palladium on activated charcoal; hydrogen; benzotriazol-1-ol; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c3cc48850k