Technology Process of C33H39N4OP
There total 11 articles about C33H39N4OP which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / dichloromethane / 10 h / 0 - 20 °C
2: acetonitrile / 24 h / Reflux
3: hydrogenchloride; water / ethanol / 10 h / Reflux
4: Hexamethylphosphorous triamide; phosphorus trichloride / acetonitrile / 0 - 20 °C / Inert atmosphere
5: potassium tert-butylate / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
With
hydrogenchloride; potassium tert-butylate; water; triethylamine; Hexamethylphosphorous triamide; phosphorus trichloride;
In
tetrahydrofuran; ethanol; dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2011.01.041
- Guidance literature:
-
Multi-step reaction with 4 steps
1: acetonitrile / 24 h / Reflux
2: hydrogenchloride; water / ethanol / 10 h / Reflux
3: Hexamethylphosphorous triamide; phosphorus trichloride / acetonitrile / 0 - 20 °C / Inert atmosphere
4: potassium tert-butylate / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere
With
hydrogenchloride; potassium tert-butylate; water; Hexamethylphosphorous triamide; phosphorus trichloride;
In
tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1016/j.tetlet.2011.01.041