methyl 7-(4-fluorophenyl)-7-<2-hydroxy-5-(methoxymethyl)-3,4,6-trimethylphenyl>heptanoate

Base Information

Chemical Name:methyl 7-(4-fluorophenyl)-7-<2-hydroxy-5-(methoxymethyl)-3,4,6-trimethylphenyl>heptanoate
CAS No.:121099-97-6
Molecular Formula:C₂₅H₃₃FO₄
Molecular Weight:416.533
Hs Code.:

Synonyms:methyl 7-(4-fluorophenyl)-7-<2-hydroxy-5-(methoxymethyl)-3,4,6-trimethylphenyl>heptanoate

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Chemical Property of methyl 7-(4-fluorophenyl)-7-<2-hydroxy-5-(methoxymethyl)-3,4,6-trimethylphenyl>heptanoate

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Technology Process of methyl 7-(4-fluorophenyl)-7-<2-hydroxy-5-(methoxymethyl)-3,4,6-trimethylphenyl>heptanoate

There total 5 articles about methyl 7-(4-fluorophenyl)-7-<2-hydroxy-5-(methoxymethyl)-3,4,6-trimethylphenyl>heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 697-82-5
2,3,5-trimethylphenol

: 121099-97-6
methyl 7-(4-fluorophenyl)-7-<2-hydroxy-5-(methoxymethyl)-3,4,6-trimethylphenyl>heptanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / BF₃*Et₂O / 1,2-dichloro-ethane / 6 h / 60 °C

2: 97 percent / TiCl₄ / CH₂Cl₂ / 0.33 h / -12 - -10 °C

3: 70 percent / NaBH₄ / tetrahydrofuran / 2 h / Ambient temperature

4: 70 percent / conc. H₂SO₄ / 0.5 h / Ambient temperature

With sodium tetrahydroborate; sulfuric acid; boron trifluoride diethyl etherate; titanium tetrachloride; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm00090a009

Reference yield:

: 103187-28-6
7-(4-fluorophenyl)-7-hydroxyheptanoic acid

: 121099-97-6
methyl 7-(4-fluorophenyl)-7-<2-hydroxy-5-(methoxymethyl)-3,4,6-trimethylphenyl>heptanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / BF₃*Et₂O / 1,2-dichloro-ethane / 6 h / 60 °C

2: 97 percent / TiCl₄ / CH₂Cl₂ / 0.33 h / -12 - -10 °C

3: 70 percent / NaBH₄ / tetrahydrofuran / 2 h / Ambient temperature

4: 70 percent / conc. H₂SO₄ / 0.5 h / Ambient temperature

With sodium tetrahydroborate; sulfuric acid; boron trifluoride diethyl etherate; titanium tetrachloride; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm00090a009

Reference yield:

: 121099-61-4
7-(4-fluorophenyl)-7-(2-hydroxy-3,4,6-trimethylphenyl)heptanoic acid

: 121099-97-6
methyl 7-(4-fluorophenyl)-7-<2-hydroxy-5-(methoxymethyl)-3,4,6-trimethylphenyl>heptanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / TiCl₄ / CH₂Cl₂ / 0.33 h / -12 - -10 °C

2: 70 percent / NaBH₄ / tetrahydrofuran / 2 h / Ambient temperature

3: 70 percent / conc. H₂SO₄ / 0.5 h / Ambient temperature

With sodium tetrahydroborate; sulfuric acid; titanium tetrachloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00090a009