1,2,4,5,8,9-hexabutoxy-3,3,10,10-tetraphenyl-6-diphenylsilyltriphenyleno[1,12-bcd:4,5-b'c'd']disilole

Base Information

Chemical Name:1,2,4,5,8,9-hexabutoxy-3,3,10,10-tetraphenyl-6-diphenylsilyltriphenyleno[1,12-bcd:4,5-b'c'd']disilole
CAS No.:1190956-37-6
Molecular Formula:C₇₈H₈₆O₆Si₃
Molecular Weight:1203.79
Hs Code.:

Synonyms:1,2,4,5,8,9-hexabutoxy-3,3,10,10-tetraphenyl-6-diphenylsilyltriphenyleno[1,12-bcd:4,5-b'c'd']disilole

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Chemical Property of 1,2,4,5,8,9-hexabutoxy-3,3,10,10-tetraphenyl-6-diphenylsilyltriphenyleno[1,12-bcd:4,5-b'c'd']disilole

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Technology Process of 1,2,4,5,8,9-hexabutoxy-3,3,10,10-tetraphenyl-6-diphenylsilyltriphenyleno[1,12-bcd:4,5-b'c'd']disilole

There total 1 articles about 1,2,4,5,8,9-hexabutoxy-3,3,10,10-tetraphenyl-6-diphenylsilyltriphenyleno[1,12-bcd:4,5-b'c'd']disilole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1190956-36-5
6-bromo-1,2,4,5,8,9-hexabutoxy-3,3,10,10-tetraphenyltriphenyleno[1,12-bcd:4,5-b'c'd']disilole

: 775-12-2
diphenylsilane

: 1190956-37-6
1,2,4,5,8,9-hexabutoxy-3,3,10,10-tetraphenyl-6-diphenylsilyltriphenyleno[1,12-bcd:4,5-b'c'd']disilole

Guidance literature:: 6-bromo-1,2,4,5,8,9-hexabutoxy-3,3,10,10-tetraphenyltriphenyleno[1,12-bcd:4,5-b'c'd']disilole; With tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃; Inert atmosphere;

diphenylsilane; In diethyl ether; pentane; at -78 ℃; for 20h; Reflux; Inert atmosphere;
DOI:10.1021/ja906566r

Reference yield: 31.0%

: 1190956-37-6
1,2,4,5,8,9-hexabutoxy-3,3,10,10-tetraphenyl-6-diphenylsilyltriphenyleno[1,12-bcd:4,5-b'c'd']disilole

: 1190956-38-7
C₇₈H₈₄O₆Si₃

: 1217974-67-8
C₆₆H₇₆O₆Si₂

Guidance literature:: With 2,6-dimethylpyridine; trityl tetrakis(pentafluorophenyl)borate; In dichloromethane; at 30 ℃; for 25h; Inert atmosphere;
DOI:10.1039/c0dt00136h

Reference yield: 18.0%

: 1190956-37-6
1,2,4,5,8,9-hexabutoxy-3,3,10,10-tetraphenyl-6-diphenylsilyltriphenyleno[1,12-bcd:4,5-b'c'd']disilole

: 1190956-38-7
C₇₈H₈₄O₆Si₃

Guidance literature:: With 2,6-dimethylpyridine; trityl tetrakis(pentafluorophenyl)borate; In dichloromethane; at 20 ℃; for 25h; Inert atmosphere;
DOI:10.1021/ja906566r