ethyl 3-(4-benzyloxyphenyl)-3-tert-butoxycarboxamido-2-hydroxypropanoate

Base Information

Chemical Name:ethyl 3-(4-benzyloxyphenyl)-3-tert-butoxycarboxamido-2-hydroxypropanoate
CAS No.:862890-45-7
Molecular Formula:C₂₃H₂₉NO₆
Molecular Weight:415.486
Hs Code.:

Synonyms:ethyl 3-(4-benzyloxyphenyl)-3-tert-butoxycarboxamido-2-hydroxypropanoate

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Chemical Property of ethyl 3-(4-benzyloxyphenyl)-3-tert-butoxycarboxamido-2-hydroxypropanoate

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Technology Process of ethyl 3-(4-benzyloxyphenyl)-3-tert-butoxycarboxamido-2-hydroxypropanoate

There total 1 articles about ethyl 3-(4-benzyloxyphenyl)-3-tert-butoxycarboxamido-2-hydroxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 846066-98-6
ethyl 3-azido-3-(4-(benzyloxy)phenyl)-2-hydroxypropanoate

: 862890-45-7
ethyl 3-(4-benzyloxyphenyl)-3-tert-butoxycarboxamido-2-hydroxypropanoate

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; water; at 20 ℃; for 12h;

Reference yield: 87.0%

: 862890-45-7
ethyl 3-(4-benzyloxyphenyl)-3-tert-butoxycarboxamido-2-hydroxypropanoate

: (4R,5S)-4-(4-Benzyloxy-phenyl)-2-oxo-oxazolidine-5-carboxylic acid ethyl ester

Guidance literature:: With triethylamine; p-toluenesulfonyl chloride; In acetonitrile; for 4h; Heating;

Reference yield:

: 862890-45-7
ethyl 3-(4-benzyloxyphenyl)-3-tert-butoxycarboxamido-2-hydroxypropanoate

: (4R,5S)-4-(4-Hydroxy-phenyl)-2-oxo-oxazolidine-5-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / Et₃N; tosyl chloride / acetonitrile / 4 h / Heating

2: 95 percent / H₂ / Pd/C

With hydrogen; triethylamine; p-toluenesulfonyl chloride; palladium on activated charcoal; In acetonitrile;