N-[5-(1,1-dimethyl-1-ethyl)-5-hexen-2-oxy]-4-(p-chlorophenyl)thiazole-2(3H)thione

Base Information

Chemical Name:N-[5-(1,1-dimethyl-1-ethyl)-5-hexen-2-oxy]-4-(p-chlorophenyl)thiazole-2(3H)thione
CAS No.:781665-90-5
Molecular Formula:C₁₉H₂₄ClNOS₂
Molecular Weight:381.991
Hs Code.:

Synonyms:N-[5-(1,1-dimethyl-1-ethyl)-5-hexen-2-oxy]-4-(p-chlorophenyl)thiazole-2(3H)thione

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Chemical Property of N-[5-(1,1-dimethyl-1-ethyl)-5-hexen-2-oxy]-4-(p-chlorophenyl)thiazole-2(3H)thione

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Technology Process of N-[5-(1,1-dimethyl-1-ethyl)-5-hexen-2-oxy]-4-(p-chlorophenyl)thiazole-2(3H)thione

There total 3 articles about N-[5-(1,1-dimethyl-1-ethyl)-5-hexen-2-oxy]-4-(p-chlorophenyl)thiazole-2(3H)thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: N-(hydroxy)-4-(p-chlorophenyl)thiazole-2(3H)-thione tetraethylammonium salt

: 781666-06-6
5-(1,1-dimethyl-1-ethyl)-5-hexene-2-yl p-toluenesulfonate

: 781665-90-5
N-[5-(1,1-dimethyl-1-ethyl)-5-hexen-2-oxy]-4-(p-chlorophenyl)thiazole-2(3H)thione

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ja049010g

Reference yield:

: 139367-18-3
2,2-dimethyl-6-hydroxy-3-heptanone

: 781665-90-5
N-[5-(1,1-dimethyl-1-ethyl)-5-hexen-2-oxy]-4-(p-chlorophenyl)thiazole-2(3H)thione

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butoxide / tetrahydrofuran / 1 h / 20 °C

1.2: 49 percent / tetrahydrofuran / 48 h / 40 °C

2.1: 90 percent / 1,4-diazabicyclo[2.2.2]octane / CH₂Cl₂ / 3 h / 20 °C

3.1: 64 percent / dimethylformamide / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; potassium tert-butylate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1.2: Wittig reaction;
DOI:10.1021/ja049010g

Reference yield:

: 781666-05-5
5-(1,1-dimethyl-1-ethyl)-5-hexene-2-ol

: 781665-90-5
N-[5-(1,1-dimethyl-1-ethyl)-5-hexen-2-oxy]-4-(p-chlorophenyl)thiazole-2(3H)thione

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 1,4-diazabicyclo[2.2.2]octane / CH₂Cl₂ / 3 h / 20 °C

2: 64 percent / dimethylformamide / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja049010g