5,5'-ureylene-di-(1-(3-(3-(pyrrolidin-1-yl)propanamido)-phenyl)-3-phenylurea)

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Chemical Name:5,5'-ureylene-di-(1-(3-(3-(pyrrolidin-1-yl)propanamido)-phenyl)-3-phenylurea)
CAS No.:1070978-30-1
Molecular Formula:C₄₁H₄₈N₁₀O₅
Molecular Weight:760.896
Hs Code.:

Synonyms:5,5'-ureylene-di-(1-(3-(3-(pyrrolidin-1-yl)propanamido)-phenyl)-3-phenylurea)

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Chemical Property of 5,5'-ureylene-di-(1-(3-(3-(pyrrolidin-1-yl)propanamido)-phenyl)-3-phenylurea)

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Technology Process of 5,5'-ureylene-di-(1-(3-(3-(pyrrolidin-1-yl)propanamido)-phenyl)-3-phenylurea)

There total 6 articles about 5,5'-ureylene-di-(1-(3-(3-(pyrrolidin-1-yl)propanamido)-phenyl)-3-phenylurea) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1070979-19-9
1-(3-(3-(pyrrolidin-1-yl)propanamido)phenyl)-3-(3-aminophenyl)urea

: 530-62-1
1,1'-carbonyldiimidazole

: 1070978-30-1
5,5'-ureylene-di-(1-(3-(3-(pyrrolidin-1-yl)propanamido)-phenyl)-3-phenylurea)

Guidance literature:: In tetrahydrofuran; at 75 ℃; for 0.333333h; under 0 Torr; Microwave irradiation;

Reference yield:

: 851651-86-0
N-(3-nitrophenyl)-3-(pyrrolidin-1-yl)propanamide

: 1070978-30-1
5,5'-ureylene-di-(1-(3-(3-(pyrrolidin-1-yl)propanamido)-phenyl)-3-phenylurea)

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium formate / palladium on activated charcoal / methanol / 20 °C

2.1: diphenyl phosphoryl azide; triethylamine / toluene / 0.5 h / 20 °C

2.2: 16 h / 115 °C

3.1: ammonium formate / palladium on activated charcoal / ethanol / 0.17 h / 120 °C / 5250.53 Torr / Microwave irradiation

4.1: tetrahydrofuran / 0.33 h / 75 °C / 0 Torr / Microwave irradiation

With diphenyl phosphoryl azide; ammonium formate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; toluene;

Reference yield:

: 851651-87-1
N-(3-aminophenyl)-3-(pyrrolidin-1-yl)propanamide

: 1070978-30-1
5,5'-ureylene-di-(1-(3-(3-(pyrrolidin-1-yl)propanamido)-phenyl)-3-phenylurea)

Guidance literature:: Multi-step reaction with 3 steps

1.1: diphenyl phosphoryl azide; triethylamine / toluene / 0.5 h / 20 °C

1.2: 16 h / 115 °C

2.1: ammonium formate / palladium on activated charcoal / ethanol / 0.17 h / 120 °C / 5250.53 Torr / Microwave irradiation

3.1: tetrahydrofuran / 0.33 h / 75 °C / 0 Torr / Microwave irradiation

With diphenyl phosphoryl azide; ammonium formate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; toluene;